Germane, dichloro(chloromethyl)[(3-methylphenyl)methyl]-

Base Information

Chemical Name:Germane, dichloro(chloromethyl)[(3-methylphenyl)methyl]-
CAS No.:395643-94-4
Molecular Formula:C₉H₁₁Cl₃Ge
Molecular Weight:298.135
Hs Code.:

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Chemical Property of Germane, dichloro(chloromethyl)[(3-methylphenyl)methyl]-

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Technology Process of Germane, dichloro(chloromethyl)[(3-methylphenyl)methyl]-

There total 1 articles about Germane, dichloro(chloromethyl)[(3-methylphenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 620-19-9
1-chloromethyl-3-methyl-benzene

: 21572-18-9
trichloro(chloromethyl)germane

: 395643-94-4
dichloro(chloromethyl)(3-methylbenzyl)germane

Guidance literature:: With Mg; In diethyl ether; (N2); addn. dropwise of soln. of C8H9Cl in Et2O to suspn. of Mg in Et2O at -10°C for 30 min; stirring for 1 h at this temp.; addn. to stirred soln. of GeCH2Cl3 in Et2O at room temp. for 30 min, stirring at room temp. for 16 h, reflux for 1 h; addn. of n-pentane, pptn., filtration, washing with n-pentane, combination of filtrate and wash solns., removal of solvent under reduced pressure, distn. in vac., elem. anal.;
DOI:10.1021/om010816o

Reference yield: 90.0%

: 395643-94-4
dichloro(chloromethyl)(3-methylbenzyl)germane

: 917-54-4
methyllithium

: 395643-95-5
(chloromethyl)dimethyl(3-methylbenzyl)germane

Guidance literature:: In diethyl ether; (N2); addn. dropwise of soln. of CH3Li in Et2O to soln. of GeC9H11Cl3 inEt2O at -10°C for 45 min, stirring for 1 h at this temp., warmin g to room temp., stirring for 3 h; removal of solvent under reduced pressure, distn. in vac., elem. anal.;
DOI:10.1021/om010816o