2(1H)-Azecinone, octahydro-9-methyl-1-(phenylmethyl)-

Base Information

Chemical Name:2(1H)-Azecinone, octahydro-9-methyl-1-(phenylmethyl)-
CAS No.:399031-54-0
Molecular Formula:C17H25NO
Molecular Weight:259.392
Hs Code.:

Synonyms:

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Chemical Property of 2(1H)-Azecinone, octahydro-9-methyl-1-(phenylmethyl)-

Chemical Property:

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Technology Process of 2(1H)-Azecinone, octahydro-9-methyl-1-(phenylmethyl)-

There total 6 articles about 2(1H)-Azecinone, octahydro-9-methyl-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 399031-53-9
(+/-)-hex-5-enoic acid benzyl(2'-methylpent-4'-enyl)amide

: 399031-54-0
(+/-)-benzyl-9-methylazacyclodecan-2-one

Guidance literature:: (+/-)-hex-5-enoic acid benzyl(2'-methylpent-4'-enyl)amide; Grubbs catalyst first generation; In dichloromethane; for 48h; Heating;

With hydrogen; palladium on activated charcoal; In methanol; at 18 ℃; for 24h; under 760.051 Torr; Further stages.;
DOI:10.1039/b105045c

Reference yield:

: 141192-61-2
(+/-)-2-methylpent-4-enoic acid benzylamide

: 399031-54-0
(+/-)-benzyl-9-methylazacyclodecan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / lithium aluminium hydride / tetrahydrofuran / 15 h / 0 - 18 °C

2.1: 42 percent / DMTMM / tetrahydrofuran / 15 h / 18 °C

3.1: [(Cy₃P)2Cl₂RuCHPh] / CH₂Cl₂ / 48 h / Heating

3.2: hydrogen / Pd on C / methanol / 24 h / 18 °C / 760.05 Torr

With lithium aluminium tetrahydride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b105045c

Reference yield:

: 1575-74-2
(+-)-2-methyl-pent-4-enoic acid

: 399031-54-0
(+/-)-benzyl-9-methylazacyclodecan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / DMTMM / tetrahydrofuran / 15 h / 18 °C

2.1: 99 percent / lithium aluminium hydride / tetrahydrofuran / 15 h / 0 - 18 °C

3.1: 42 percent / DMTMM / tetrahydrofuran / 15 h / 18 °C

4.1: [(Cy₃P)2Cl₂RuCHPh] / CH₂Cl₂ / 48 h / Heating

4.2: hydrogen / Pd on C / methanol / 24 h / 18 °C / 760.05 Torr

With lithium aluminium tetrahydride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b105045c