Benzene, 2-[(1S)-1,5-dimethyl-4-hexenyl]-1-(methoxymethoxy)-4-methyl-

Base Information

Chemical Name:Benzene, 2-[(1S)-1,5-dimethyl-4-hexenyl]-1-(methoxymethoxy)-4-methyl-
CAS No.:399535-10-5
Molecular Formula:C17H26O2
Molecular Weight:262.392
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 2-[(1S)-1,5-dimethyl-4-hexenyl]-1-(methoxymethoxy)-4-methyl-

Chemical Property:

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Technology Process of Benzene, 2-[(1S)-1,5-dimethyl-4-hexenyl]-1-(methoxymethoxy)-4-methyl-

There total 9 articles about Benzene, 2-[(1S)-1,5-dimethyl-4-hexenyl]-1-(methoxymethoxy)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 399535-11-6
methyl 5-hydroxy-4-(2'-methoxy-5'-methylphenyl)-(2E)-pentenoate

: 399535-10-5
2-methyl-(6S)-(2'-methoxymethyloxy-5'-methyl)phenyl-2-heptene

Guidance literature:: Multi-step reaction with 9 steps

1.1: 85 percent / pyridine / benzene / 12 h

2.1: 100 percent / H₂ / 20 percent Pd/C / methanol / 20 °C / atmospheric pressure

3.1: NaBH₄ / dimethylsulfoxide / 2 h / 80 °C

3.2: 0.745 g / LiAlH₄ / tetrahydrofuran / 3 h / 20 °C

4.1: 91 percent / AlCl₃; ethanethiol / 0.5 h / 0 °C

5.1: 65 percent / pyridine / 1 h / 20 °C

6.1: 88 percent / N,N-diisopropylethylamine / acetonitrile / 12 h / 40 °C

7.1: 93 percent / K₂CO₃ / methanol / 1 h / 20 °C

8.1: 0.06 g / pyridinium chlorochromate; Celite 545 / CH₂Cl₂ / 2 h / 20 °C

9.1: 0.016 g / n-BuLi / tetrahydrofuran; hexane / 1.5 h / 20 °C

With pyridine; sodium tetrahydroborate; n-butyllithium; aluminium trichloride; Celite; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; ethanethiol; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; dimethyl sulfoxide; acetonitrile; benzene; 9.1: Wittig reaction;
DOI:10.1016/S0957-4166(01)00447-5

Reference yield:

: 399535-02-5
methyl 5-tosyloxy-4-(2'-methoxy-5'-methylphenyl)-(2E)-pentenoate

: 399535-10-5
2-methyl-(6S)-(2'-methoxymethyloxy-5'-methyl)phenyl-2-heptene

Guidance literature:: Multi-step reaction with 8 steps

1.1: 100 percent / H₂ / 20 percent Pd/C / methanol / 20 °C / atmospheric pressure

2.1: NaBH₄ / dimethylsulfoxide / 2 h / 80 °C

2.2: 0.745 g / LiAlH₄ / tetrahydrofuran / 3 h / 20 °C

3.1: 91 percent / AlCl₃; ethanethiol / 0.5 h / 0 °C

4.1: 65 percent / pyridine / 1 h / 20 °C

5.1: 88 percent / N,N-diisopropylethylamine / acetonitrile / 12 h / 40 °C

6.1: 93 percent / K₂CO₃ / methanol / 1 h / 20 °C

7.1: 0.06 g / pyridinium chlorochromate; Celite 545 / CH₂Cl₂ / 2 h / 20 °C

8.1: 0.016 g / n-BuLi / tetrahydrofuran; hexane / 1.5 h / 20 °C

With sodium tetrahydroborate; n-butyllithium; aluminium trichloride; Celite; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; ethanethiol; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; dimethyl sulfoxide; acetonitrile; 8.1: Wittig reaction;
DOI:10.1016/S0957-4166(01)00447-5