10-(acetyloxy)-4,6,9-trimethyl-13-methylidene-12-oxodecahydro-2H-2,9-pentanofuro[2,3,4-ef][3]benzoxepin-3-yl butanoate

Base Information

Chemical Name:10-(acetyloxy)-4,6,9-trimethyl-13-methylidene-12-oxodecahydro-2H-2,9-pentanofuro[2,3,4-ef][3]benzoxepin-3-yl butanoate
CAS No.:74145-71-4
Molecular Formula:C₂₆H₃₈O₇
Molecular Weight:462.584
Hs Code.:

Synonyms:

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(acetyloxy)-4,6,9-trimethyl-13-methylidene-12-oxodecahydro-2H-2,9-pentanofuro[2,3,4-ef][3]benzoxepin-3-yl butanoate

Chemical Property:

Vapor Pressure:3.49E-12mmHg at 25°C
Boiling Point:550.9°Cat760mmHg
Flash Point:233.8°C
Density:1.17g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 10-(acetyloxy)-4,6,9-trimethyl-13-methylidene-12-oxodecahydro-2H-2,9-pentanofuro[2,3,4-ef][3]benzoxepin-3-yl butanoate

There total 2 articles about 10-(acetyloxy)-4,6,9-trimethyl-13-methylidene-12-oxodecahydro-2H-2,9-pentanofuro[2,3,4-ef][3]benzoxepin-3-yl butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74145-70-3
asbestinin-5

: 74145-71-4
asbestinin-4

Guidance literature:: With manganese(IV) oxide; In chloroform; for 2h; Ambient temperature;
DOI:10.1021/ja00535a047

Reference yield:

: 74145-72-5
asbestinin-3

: 74145-71-4
asbestinin-4

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 48 h / Ambient temperature

2: 65 percent / O₂, methylene blue / CH₂Cl₂ / 12 h / 0 - 10 °C / Irradiation

3: 80 percent / MnO₂ / CHCl₃ / 2 h / Ambient temperature

With pyridine; manganese(IV) oxide; oxygen; methylene blue; In dichloromethane; chloroform;
DOI:10.1021/ja00535a047

Reference yield:

: 74145-71-4
asbestinin-4

: 75961-67-0
asbestinin-5-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / LiAlH₄ / diethyl ether / 0.5 h / -78 °C

2: 53 percent / pyridine / 18 h / Ambient temperature

With lithium aluminium tetrahydride; In pyridine; diethyl ether;
DOI:10.1021/jo00318a023