Pyridine, 2-(3,5-diphenyl-1H-pyrrol-2-yl)-

Base Information

Chemical Name:Pyridine, 2-(3,5-diphenyl-1H-pyrrol-2-yl)-
CAS No.:402500-01-0
Molecular Formula:C21H16N2
Molecular Weight:296.371
Hs Code.:
Mol file:402500-01-0.mol

Synonyms:

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Chemical Property of Pyridine, 2-(3,5-diphenyl-1H-pyrrol-2-yl)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Pyridine, 2-(3,5-diphenyl-1H-pyrrol-2-yl)-

There total 1 articles about Pyridine, 2-(3,5-diphenyl-1H-pyrrol-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: 402500-01-0
2-(3,5-diphenyl-1H-pyrrol-2-yl)pyridine

Guidance literature:: With toluene-4-sulfonic acid; In xylene; at 170 ℃; for 16h;
DOI:10.1021/ol017147v

Reference yield: 99.0%

: 557-20-0
diethylzinc

: 108-88-3,15644-74-3,16713-13-6
toluene

: 402500-01-0
2-(3,5-diphenyl-1H-pyrrol-2-yl)pyridine

: bis(3,5-diphenyl-2-(2'-pyridyl)pyrrolyl)zinc*toluene

Guidance literature:: In tetrahydrofuran; (N2); addn. of zinc compd. to a soln. of ligand in THF; evapn., recrystn. (hexanes/toluene 6:1, -35°C);
DOI:10.1039/b315523d

Reference yield: 92.0%

: 52586-35-3,60817-02-9
[(S(CH₃)2)PtCl₂]2

: 402500-01-0
2-(3,5-diphenyl-1H-pyrrol-2-yl)pyridine

: 1165813-34-2
[(3,5-diphenyl-2-(2-piridyl)pyrrolide)Pt(SMe₂)Cl]

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; byproducts: LiCl; (N2); std. Schlenk technique; Li compd. was added to soln. of ligand in THF; stirred for 30 min; soln. of Pt complex (0.5 equiv.) in THF was added; stirred for 1 h; evapd. (vac.); dissolved in C6H6; filtered through Celite; evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om9002686