Uridine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-deoxy-3-[4-(1,1-dimethyleth yl)benzoyl]-2'-methyl-

Base Information

Chemical Name:Uridine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-deoxy-3-[4-(1,1-dimethyleth yl)benzoyl]-2'-methyl-
CAS No.:402518-09-6
Molecular Formula:C42H44N2O8
Molecular Weight:704.82
Hs Code.:

Synonyms:

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Chemical Property of Uridine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-deoxy-3-[4-(1,1-dimethyleth yl)benzoyl]-2'-methyl-

Chemical Property:

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Technology Process of Uridine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-deoxy-3-[4-(1,1-dimethyleth yl)benzoyl]-2'-methyl-

There total 4 articles about Uridine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-2'-deoxy-3-[4-(1,1-dimethyleth yl)benzoyl]-2'-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 402518-06-3
(2'R)-2'-deoxy-2'-C-methyl-N³-(4-t-butylbenzoyl) uridine

: 402518-09-6
5'-O-dimethoxytrityl-(2'R)-2'-deoxy-2'-C-methyl-N³-(4-t-butylbenzoyl) uridine

Guidance literature:: With triethylamine; In pyridine;
DOI:10.1016/S0040-4020(01)00745-1

Reference yield:

: 1710-98-1
p-tert-butyl benzoyl chloride

: 402518-09-6
5'-O-dimethoxytrityl-(2'R)-2'-deoxy-2'-C-methyl-N³-(4-t-butylbenzoyl) uridine

Guidance literature:: Multi-step reaction with 3 steps

1: 12 mg / tetrabutylammonium bromide; Na₂CO₃ / CH₂Cl₂; H₂O / 20 °C

2: 97 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h

3: 63 percent / Et₃N / pyridine

With tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium carbonate; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; water;
DOI:10.1016/S0040-4020(01)00745-1

Reference yield:

: 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-deoxy-2'-C-methyluridine

: 402518-09-6
5'-O-dimethoxytrityl-(2'R)-2'-deoxy-2'-C-methyl-N³-(4-t-butylbenzoyl) uridine

Guidance literature:: Multi-step reaction with 3 steps

1: 12 mg / tetrabutylammonium bromide; Na₂CO₃ / CH₂Cl₂; H₂O / 20 °C

2: 97 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h

3: 63 percent / Et₃N / pyridine

With tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium carbonate; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; water;
DOI:10.1016/S0040-4020(01)00745-1