Technology Process of 1,3-Dioxo-1h-benzo[de]isoquinolin-2(3h)-yl trifluoromethanesulfonate
There total 3 articles about 1,3-Dioxo-1h-benzo[de]isoquinolin-2(3h)-yl trifluoromethanesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-hydroxy-1,8-naphthalenedicarboximide; trifluoromethane sulfonyl chloride;
In
5,5-dimethyl-1,3-cyclohexadiene;
at 10 ℃;
for 7h;
With
sodium hydroxide;
In
5,5-dimethyl-1,3-cyclohexadiene; water;
for 0.5h;
Solvent;
Temperature;
- Guidance literature:
-
1,8-Naphthalic anhydride;
With
pyridine; hydroxylamine hydrochloride;
at 100 ℃;
for 10h;
With
hydrogenchloride;
In
water;
trifluoromethylsulfonic anhydride;
With
pyridine;
at 0 - 25 ℃;
for 2h;
- Guidance literature:
-
With
pyridine; hydroxylamine hydrochloride;
at 115 ℃;
for 5h;
With
pyridine;
In
dichloromethane;
at 40 ℃;
for 6.25h;
Cooling with ice;
