4-hydroxy-2,3-dimethylphenyl thiocyanate

Base Information

• Chemical Name: 4-hydroxy-2,3-dimethylphenyl thiocyanate
• CAS No.: 6186-84-1
• Molecular Formula: C9H9NOS
• Molecular Weight: 179.243
• Mol file: 6186-84-1.mol

Synonyms:

Chemical Property of 4-hydroxy-2,3-dimethylphenyl thiocyanate

Chemical Property:

• Vapor Pressure: 0.000796mmHg at 25°C
• Boiling Point: 296.8°Cat760mmHg
• Flash Point: 133.3°C
• Density: 1.24g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-hydroxy-2,3-dimethylphenyl thiocyanate

There total 2 articles about 4-hydroxy-2,3-dimethylphenyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ammonium thiocyanate + 2,3-Dimethylphenol (526-75-0) → 2,3-dimethyl-4-thiocyanatophenol (6186-84-1)

Guidance literature:

With dipotassium peroxodisulfate; In dichloromethane; at 20 ℃; for 4h; regioselective reaction;

DOI:10.1016/j.tetlet.2016.12.043

Reference yield:

→ 2,3-dimethyl-4-thiocyanatophenol (6186-84-1)

Guidance literature:

2,3-Dimethyl-phenol, NaSCN;

upstream raw materials:

2,3-Dimethylphenol