4-({4-[(2-chloro-4-nitrophenoxy)methyl]benzyl}oxy)benzenesulfonyl fluoride

Base Information

• Chemical Name: 4-({4-[(2-chloro-4-nitrophenoxy)methyl]benzyl}oxy)benzenesulfonyl fluoride
• CAS No.: 31185-39-4
• Molecular Formula: C₂₀H₁₅ClFNO₆S
• Molecular Weight: 451.86
• Mol file: 31185-39-4.mol

Synonyms:Benzenesulfonylfluoride, p-[[p-[(2-chloro-4-nitrophenoxy)methyl]benzyl]oxy]- (8CI); NSC 212397

Chemical Property of 4-({4-[(2-chloro-4-nitrophenoxy)methyl]benzyl}oxy)benzenesulfonyl fluoride

Chemical Property:

• Vapor Pressure: 1.72E-13mmHg at 25°C
• Boiling Point: 594.9°Cat760mmHg
• Flash Point: 313.6°C
• Density: 1.441g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-({4-[(2-chloro-4-nitrophenoxy)methyl]benzyl}oxy)benzenesulfonyl fluoride

There total 3 articles about 4-({4-[(2-chloro-4-nitrophenoxy)methyl]benzyl}oxy)benzenesulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis(bromomethyl)benzene (623-24-5) → α-(2-Chlor-4-nitrophenoxy)-α'-(p-fluorsulfonyl-phenoxy)-p-xylol (31185-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: K₂CO₃ / dimethylformamide / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jm00300a029

Reference yield:

2-chloro-4-nitrophenol (619-08-9) → α-(2-Chlor-4-nitrophenoxy)-α'-(p-fluorsulfonyl-phenoxy)-p-xylol (31185-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: K₂CO₃ / dimethylformamide / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jm00300a029

Reference yield:

1-(4-Bromomethyl-benzyloxy)-2-chloro-4-nitro-benzene (31191-41-0) + 4-hydroxybenzene-1-sulfonyl fluoride (368-87-6) → α-(2-Chlor-4-nitrophenoxy)-α'-(p-fluorsulfonyl-phenoxy)-p-xylol (31185-39-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jm00300a029

upstream raw materials:

1-(4-Bromomethyl-benzyloxy)-2-chloro-4-nitro-benzene

4-hydroxybenzene-1-sulfonyl fluoride

1,4-bis(bromomethyl)benzene

2-chloro-4-nitrophenol

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