Technology Process of 6-Methylcholanthrene
There total 8 articles about 6-Methylcholanthrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydrazine;
In
diethylene glycol;
for 12h;
Heating;
DOI:10.1021/jo00299a018
- Guidance literature:
-
Multi-step reaction with 5 steps
1: HCl / ethyl acetate
2: 79 percent / dimethylsulfoxide / 0.67 h / 70 °C
3: 85 percent / aq. KOH / ethane-1,2-diol / 24 h / Heating
4: 16 percent / HF / 12 h / Ambient temperature
5: 46 percent / H2NNH2, KOH / bis-(2-hydroxy-ethyl) ether / 12 h / Heating
With
hydrogenchloride; potassium hydroxide; hydrogen fluoride; hydrazine;
In
ethylene glycol; dimethyl sulfoxide; ethyl acetate; diethylene glycol;
DOI:10.1021/jo00299a018
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 79 percent / dimethylsulfoxide / 0.67 h / 70 °C
2: 85 percent / aq. KOH / ethane-1,2-diol / 24 h / Heating
3: 16 percent / HF / 12 h / Ambient temperature
4: 46 percent / H2NNH2, KOH / bis-(2-hydroxy-ethyl) ether / 12 h / Heating
With
potassium hydroxide; hydrogen fluoride; hydrazine;
In
ethylene glycol; dimethyl sulfoxide; diethylene glycol;
DOI:10.1021/jo00299a018
