2,5-dimethyl-3H-1,3-benzazaphosphole

Base Information

Chemical Name:2,5-dimethyl-3H-1,3-benzazaphosphole
CAS No.:404578-27-4
Molecular Formula:C9H10NP
Molecular Weight:163.159
Hs Code.:
DSSTox Substance ID:DTXSID90422530
Nikkaji Number:J1.642.834E
Wikidata:Q82234481
Mol file:404578-27-4.mol

Synonyms:2,5-dimethyl-3H-1,3-benzazaphosphole;404578-27-4;DTXSID90422530;2,5-Dimethyl-1H-1,3-benzazaphosphole

Suppliers and Price of 2,5-dimethyl-3H-1,3-benzazaphosphole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-dimethyl-3H-1,3-benzazaphosphole

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:163.055086321
Heavy Atom Count:11
Complexity:149

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)N=C(P2)C

Technology Process of 2,5-dimethyl-3H-1,3-benzazaphosphole

There total 2 articles about 2,5-dimethyl-3H-1,3-benzazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 2-acetamido-5-methylbenzenephosphonic acid diethylester

: 404578-27-4
2,5-dimethyl-1H-1,3-benzazaphosphole

: ethyl-(4-methyl-2-phosphanyl-phenyl)-amine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 15 - 20 ℃; for 24h;
DOI:10.1016/S0040-4020(01)01019-5

Reference yield:

: 131543-46-9,107-22-2
Glyoxal

: 152435-11-5
4-methyl-2-phosphanylaniline

: 1395459-82-1
5-methyl-1H-1,3-benzazaphosphole

: 106-49-0,12221-03-3
p-toluidine

: 404578-27-4
2,5-dimethyl-1H-1,3-benzazaphosphole

Guidance literature:: In water; toluene;
DOI:10.1002/ejic.201300342

Reference yield: 64.0%

: 1174587-32-6
2-chloro-1,3-dimesityl-4,5-dimethyl-1,3,2-diazaphospholene

: 404578-27-4
2,5-dimethyl-1H-1,3-benzazaphosphole

: 1203790-86-6
C₃₁H₃₇N₃P₂

Guidance literature:: 2,5-dimethyl-1H-1,3-benzazaphosphole; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

2-chloro-1,3-dimesityl-4,5-dimethyl-1,3,2-diazaphospholene; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200901753