2-Propenoic acid, 3-[4-[[[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl][2-(1H-indol-3-yl)ethyl] amino]methyl]phenyl]-, methyl ester, (2E)-

Base Information

Chemical Name:2-Propenoic acid, 3-[4-[[[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl][2-(1H-indol-3-yl)ethyl] amino]methyl]phenyl]-, methyl ester, (2E)-
CAS No.:404951-56-0
Molecular Formula:C29H40N2O3Si
Molecular Weight:492.734
Hs Code.:
Mol file:404951-56-0.mol

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Chemical Property of 2-Propenoic acid, 3-[4-[[[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl][2-(1H-indol-3-yl)ethyl] amino]methyl]phenyl]-, methyl ester, (2E)-

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Technology Process of 2-Propenoic acid, 3-[4-[[[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl][2-(1H-indol-3-yl)ethyl] amino]methyl]phenyl]-, methyl ester, (2E)-

There total 1 articles about 2-Propenoic acid, 3-[4-[[[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl][2-(1H-indol-3-yl)ethyl] amino]methyl]phenyl]-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 404951-55-9
(2E)-3-[4-[[[2-(1H-indol-3-yl)ethyl]amino]methyl]phenyl]-2-propenoic acid methyl ester

: 404951-56-0
3-[4-({[2-(tert-butyldimethylsilanyloxy)-ethyl]-[2-(1H-indol-3-yl)-ethyl]-amino}-methyl)-phenyl]-(2E)-2-propenoic acid methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 - 55 ℃; for 24h;

Reference yield: 79.0%

: 404951-56-0
3-[4-({[2-(tert-butyldimethylsilanyloxy)-ethyl]-[2-(1H-indol-3-yl)-ethyl]-amino}-methyl)-phenyl]-(2E)-2-propenoic acid methyl ester

: 865999-79-7
3-[4-({[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-[2-(1H-indol-3-yl)ethyl]-amino}-methyl)-phenyl]acrylic acid

Guidance literature:: 3-[4-({[2-(tert-butyldimethylsilanyloxy)-ethyl]-[2-(1H-indol-3-yl)-ethyl]-amino}-methyl)-phenyl]-(2E)-2-propenoic acid methyl ester; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 24h;

With hydrogenchloride; In water; pH=5 - 6;