4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one

Base Information

Chemical Name:4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one
CAS No.:60263-15-2
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:

Synonyms:4-Hydroxy-2-isopropyl-4,7-dimethyl-1(4H)-naphthalenone

Suppliers and Price of 4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one

Chemical Property:

Vapor Pressure:1.03E-06mmHg at 25°C
Boiling Point:388°C at 760 mmHg
Flash Point:165.7°C
Density:1.108g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one

There total 7 articles about 4-hydroxy-4,7-dimethyl-2-(propan-2-yl)naphthalen-1(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 60263-10-7
2-Isopropyl-4,7-dimethyl-1-naphthalinol

: 60263-15-2
4-Hydroxy-2-isopropyl-4,7-dimethyl-1(4H)-naphthalinon

Guidance literature:: With potassiuim nitrosodisulfonate; sodium acetate; In diethyl ether; water; acetone; for 24h; Ambient temperature;

Reference yield:

: 78309-97-4
α-Isopropyl-4-methyl-γ-oxobenzolbutansaeure

: 60263-15-2
4-Hydroxy-2-isopropyl-4,7-dimethyl-1(4H)-naphthalinon

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / diethyl ether / 3 h / Heating

2: 88 percent / H₂ / PtO₂ / methanol

3: 1) SOCl₂, 2) AlCl₃ / 1) reflux, 1 h, 2) benzene, ligroine, 55 deg C

4: trimethylphenylammonium perbromide / tetrahydrofuran / 0.5 h / Ambient temperature

5: 78 percent / LiBr, Li₂CO₃ / dimethylformamide / 3 h / Heating

6: 21 percent / Fremy salt, 1N NaOAc / diethyl ether; H₂O; acetone / 24 h / Ambient temperature

With aluminium trichloride; thionyl chloride; potassiuim nitrosodisulfonate; hydrogen; sodium acetate; phenyltrimethylammonium tribromide; lithium carbonate; lithium bromide; platinum(IV) oxide; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 78309-98-5
4,5-Dihydro-3-isopropyl-5-methyl-5-(4-methylphenyl)-2(3H)-furanon

: 60263-15-2
4-Hydroxy-2-isopropyl-4,7-dimethyl-1(4H)-naphthalinon

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / H₂ / PtO₂ / methanol

2: 1) SOCl₂, 2) AlCl₃ / 1) reflux, 1 h, 2) benzene, ligroine, 55 deg C

3: trimethylphenylammonium perbromide / tetrahydrofuran / 0.5 h / Ambient temperature

4: 78 percent / LiBr, Li₂CO₃ / dimethylformamide / 3 h / Heating

5: 21 percent / Fremy salt, 1N NaOAc / diethyl ether; H₂O; acetone / 24 h / Ambient temperature

With aluminium trichloride; thionyl chloride; potassiuim nitrosodisulfonate; hydrogen; sodium acetate; phenyltrimethylammonium tribromide; lithium carbonate; lithium bromide; platinum(IV) oxide; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide; acetone;