N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER
CAS No.:405058-67-5
Molecular Formula:C10H13NO3
Molecular Weight:195.21500
Hs Code.:
Mol file:405058-67-5.mol

Synonyms:N-Oxide-2,4-dimethyl-3-pyridine carboxylic acid ethyl ester;2,4-dimethyl-1-oxy-nicotinic acid ethyl ester;

Suppliers and Price of N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER 95.00%
5G
$ 1976.78

American Custom Chemicals Corporation
N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER 95.00%
1G
$ 945.95

Total 2 raw suppliers

Chemical Property of N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Vapor Pressure:4.12E-05mmHg at 25°C
Boiling Point:351.4oC at 760 mmHg
Flash Point:166.3oC
PSA：51.76000
Density:1.12g/cm3
LogP:1.90860

Purity/Quality:

95% ^*data from raw suppliers

N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER

There total 1 articles about N-OXIDE-2,4-DIMETHYL-3-PYRIDINE CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37669-78-6
ethyl 2,4-dimethylnicotinate

: 405058-67-5
2,4-dimethyl-1-oxy-nicotinic acid ethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 405058-67-5
2,4-dimethyl-1-oxy-nicotinic acid ethyl ester

: 871492-83-0
6-chloro-N-(R)-{3-[4-(4-methoxy-phenylamino)-piperidin-1-yl]-butyl}-2,4-dimethyl-nicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / Reflux

2: sodium hydroxide / ethanol / 90 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.133

Reference yield:

: 405058-67-5
2,4-dimethyl-1-oxy-nicotinic acid ethyl ester

: 6-Chloro-N-((R)-3-{4-[(4-methoxy-phenyl)-(4-methyl-pyridin-3-ylmethyl)-amino]-piperidin-1-yl}-butyl)-2,4-dimethyl-nicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / Reflux

2: sodium hydroxide / ethanol / 90 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.133