Phosphoric acid, dibutyl 3-methylphenyl ester

Base Information

• Chemical Name: Phosphoric acid, dibutyl 3-methylphenyl ester
• CAS No.: 40585-82-8
• Molecular Formula: C15H25O4P
• Molecular Weight: 300.335
• Mol file: 40585-82-8.mol

Synonyms:

Chemical Property of Phosphoric acid, dibutyl 3-methylphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphoric acid, dibutyl 3-methylphenyl ester

There total 2 articles about Phosphoric acid, dibutyl 3-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

3-methyl-phenol (108-39-4) + dibutyl chlorophosphate (819-43-2) → di-n-butyl m-methylphenyl phosphate (40585-82-8)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2017.04.002

Reference yield:

→ di-n-butyl m-methylphenyl phosphate (40585-82-8)

Guidance literature:

m-Kresol, 1) POCl3 (bei 110 mit KCl als Kat.), 2) Esterif mit entspr. Alkohol bei 20grad in Ggw. MgCl2;

upstream raw materials:

3-methyl-phenol

dibutyl chlorophosphate