2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-

Base Information

Chemical Name:2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-
CAS No.:40649-34-1
Molecular Formula:C13H20O2
Molecular Weight:208.301
Hs Code.:
DSSTox Substance ID:DTXSID00460165
Nikkaji Number:J1.908.365I

Synonyms:40649-34-1;2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-;3-(2-methylpropoxy)-6-prop-2-enylcyclohex-2-en-1-one;DTXSID00460165;6-allyl-3-isobutoxy-2-cyclohexen-1-one

Suppliers and Price of 2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:208.146329876
Heavy Atom Count:15
Complexity:264

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)COC1=CC(=O)C(CC1)CC=C

Technology Process of 2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)-

There total 3 articles about 2-Cyclohexen-1-one, 3-(2-methylpropoxy)-6-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 23074-59-1
3-isobutoxycyclohex-2-en-1-one

: 106-95-6
allyl bromide

: 40649-34-1
6-allyl-3-isobutoxycyclohex-2-en-1-one

Guidance literature:: 3-isobutoxycyclohex-2-en-1-one; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -80 ℃; for 1h; Inert atmosphere;

allyl bromide; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.200900447

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 40649-34-1
6-allyl-3-isobutoxycyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 110 °C / Dean-Stark

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - -10 °C / Inert atmosphere

2.2: 3 h / -78 - 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1055/s-0037-1610187