5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel-

Base Information

Chemical Name:5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel-
CAS No.:107036-07-7
Molecular Formula:C23H29 N O3
Molecular Weight:367.488
Hs Code.:

Synonyms:5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (R*,S*)-; Ketononestrol aziridine

Suppliers and Price of 5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel-

There total 4 articles about 5-Nonanone,1-(1-aziridinyl)-6,7-bis(4-hydroxyphenyl)-, (6R,7S)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 151-56-4,9002-98-6
ethyleneimine

: 107036-22-6
(6R*,7S*)-5-oxo-6,7-bis(4-hydroxyphenyl)-1-nonanyl methanesulfonate

: 107036-07-7
(6R*,7S*)-1-N-aziridinyl-6,7-bis(4-hydroxyphenyl)-5-nonanone

Guidance literature:: With triethylamine; In acetonitrile; for 20h; Ambient temperature;
DOI:10.1021/jm00388a015

Reference yield:

: 107036-19-1
(6R*,7S*)-6,7-bis<4-(tert-butyldimethylsiloxy)phenyl>-1-nonen-5-one

: 107036-07-7
(6R*,7S*)-1-N-aziridinyl-6,7-bis(4-hydroxyphenyl)-5-nonanone

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 0.67 h / 60 °C

2: 95 percent / Et₃N / tetrahydrofuran / 0.33 h / Ambient temperature

3: 60 percent / p-TsOH*H₂O / ethyl acetate / 0.33 h / 40 °C

4: 54 percent / Et₃N / acetonitrile / 20 h / Ambient temperature

With 9-borabicyclo[3.3.1]nonane dimer; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1021/jm00388a015

Reference yield:

: 107036-20-4
(6R*,7S*)-1-hydroxy-6,7-bis<4-(tert-butyldimethylsiloxy)phenyl>-5-nonanone

: 107036-07-7
(6R*,7S*)-1-N-aziridinyl-6,7-bis(4-hydroxyphenyl)-5-nonanone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Et₃N / tetrahydrofuran / 0.33 h / Ambient temperature

2: 60 percent / p-TsOH*H₂O / ethyl acetate / 0.33 h / 40 °C

3: 54 percent / Et₃N / acetonitrile / 20 h / Ambient temperature

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1021/jm00388a015