Hydrazinecarbodithioic acid, [(5-bromo-2-hydroxyphenyl)methylene]-, methyl ester

Base Information

Chemical Name:Hydrazinecarbodithioic acid, [(5-bromo-2-hydroxyphenyl)methylene]-, methyl ester
CAS No.:42183-25-5
Molecular Formula:C₉H₉BrN₂OS₂
Molecular Weight:305.219
Hs Code.:

Synonyms:

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Chemical Property of Hydrazinecarbodithioic acid, [(5-bromo-2-hydroxyphenyl)methylene]-, methyl ester

Chemical Property:

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Technology Process of Hydrazinecarbodithioic acid, [(5-bromo-2-hydroxyphenyl)methylene]-, methyl ester

There total 2 articles about Hydrazinecarbodithioic acid, [(5-bromo-2-hydroxyphenyl)methylene]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5397-03-5
hydrazinecarbodithioic acid methyl ester

: 1761-61-1
5-bromosalicyclaldehyde

: 42183-25-5
S-methyl-3-(5-bromo-2-hydroxyphenyl)methylenedithiocarbazate

Guidance literature:: In ethanol;
DOI:10.1039/DT9930001151

Reference yield:

: 42183-25-5
S-methyl-3-(5-bromo-2-hydroxyphenyl)methylenedithiocarbazate

Guidance literature:: 5-Br-Salicylaldehyd, S-Methyl-dithiocarbazat;
DOI:10.1016/S0020-1693(00)94808-4

Reference yield: 54.0%

: 288-32-4
1H-imidazole

: bis(acetylacetonate)oxidovanadium(IV)

: 42183-25-5
S-methyl 3-(5-bromo-2-hydroxyphenyl)methylenedithiocarbazate

: 506413-59-8
VO₂⁽¹⁺⁾*OC₆H₃BrCHNNCSSCH₃^(2-)*N₂C₃H₅⁽¹⁺⁾=(VO₂(OC₆H₃BrCHNNCSSCH₃)(N₂C₃H₅))

Guidance literature:: In water; acetonitrile; to MeCN soln. (VO(acac)2) was added dithiocarbazate-based Schiff base ligand in MeCN (1:1), refluxed for 10 min, and cooled to room temp., aq. soln. imidazole was added and refluxed for 1 h; soln. was filtered and kept in air for several days, filtered and concd., filtrate cooled at 4°C overnight, ppt. was filtered off, washedwith Et2O, and recrystd. from MeOH/water; elem. anal.;
DOI:10.1021/ic020438v