3-Hexen-2-ol

Base Information

• Chemical Name: 3-Hexen-2-ol
• CAS No.: 42185-97-7
• Molecular Formula: C6H12O
• Molecular Weight: 100.161
• Mol file: 42185-97-7.mol

Synonyms:

Chemical Property of 3-Hexen-2-ol

Chemical Property:

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Technology Process of 3-Hexen-2-ol

There total 1 articles about 3-Hexen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Hexen-2-one (109-49-9) → n-hexan-2-one (591-78-6) + hex-3-en-2-ol (42185-97-7)

Guidance literature:

With C₂₁H₂₉IrN₅⁽¹⁺⁾*Cl^(1-); C₂₁H₂₉IrN₅⁽¹⁺⁾*Cl^(1-); isopropyl alcohol; In benzene-d6; at 90 ℃; for 2.5h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Glovebox;

DOI:10.1016/j.ica.2020.119551

Reference yield: 99.0%

hex-3-en-2-ol (42185-97-7) → hexa-1,3-diene (592-48-3)

Guidance literature:

With HeMaRaphos; toluene-4-sulfonic acid; palladium dichloride; In tetrahydrofuran; at 125 ℃; for 8h; Reagent/catalyst; Time; Autoclave;

DOI:10.1002/anie.202008916

Reference yield:

hex-3-en-2-ol (42185-97-7) + 1-(4-acetylphenyl)diazonium tetrafluoroborate (350-47-0) → (R)-4-(4-acetylphenyl)hexan-2-one + 4-(4-acetylphenyl)hexan-2-one

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,5-bis(3-(trifluoromethyl)phenyl)penta-1,4-dien-3-one; (S)-3,3'-bis(2,4,6-triisopropylphenyl)-5,5',6,6',7,7',8,8'-octahydro-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; sodium carbonate; dimethyl sulfoxide; In diethyl ether; at 0 ℃; for 12h; Overall yield = 75 percent; enantioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.1c00152

upstream raw materials:

5-Hexen-2-one

Downstream raw materials:

hexa-1,3-diene

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