3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride (1:1), (2R,3R,4S)-

Base Information

• Chemical Name: 3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride (1:1), (2R,3R,4S)-
• CAS No.: 117770-16-8
• Molecular Formula: C₆H₁₃NO₄*ClH
• Molecular Weight: 199.634

Synonyms:3,4-Pyrrolidinediol,2-(1,2-dihydroxyethyl)-, hydrochloride, [2R-[2a(S*),3b,4b]]-; 3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride, (2R,3R,4S)- (9CI)

Chemical Property of 3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride (1:1), (2R,3R,4S)-

Chemical Property:

• Boiling Point: 448.6°Cat760mmHg
• Flash Point: 258°C
• Density: 1.492g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride (1:1), (2R,3R,4S)-

There total 28 articles about 3,4-Pyrrolidinediol,2-[(1S)-1,2-dihydroxyethyl]-, hydrochloride (1:1), (2R,3R,4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(2S,3R,4S)-1-Benzyl-2-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-pyrrolidine-3,4-diol (858656-63-0) → 1,4-dideoxy-1,4-imino-D-allitol hydrochloride (117770-16-8)

Guidance literature:

With hydrogenchloride; hydrogen; palladium dihydroxide; In methanol;

DOI:10.1016/j.tetlet.2003.11.053

Reference yield: 95.0%

(3aR,4R,6aS)-4-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole-5-carboxylic acid tert-butyl ester (603126-12-1) → 1,4-dideoxy-1,4-imino-D-allitol hydrochloride (117770-16-8)

Guidance literature:

With hydrogenchloride; In methanol; at 23 ℃; for 5h;

DOI:10.1016/j.tetasy.2006.12.023

Reference yield: 95.0%

1,4-Dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-allitol (117859-46-8) → 1,4-dideoxy-1,4-imino-D-allitol hydrochloride (117770-16-8)

Guidance literature:

With hydrogenchloride; for 24h;

upstream raw materials:

1,4-Dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-allitol

N-(tert-butoxycarbonyl)-1,4-dideoxy-1,4-imino-5,6-O-isopropylidene-D-allitol

(2S,3R,4S)-1-Benzyl-2-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-pyrrolidine-3,4-diol

(3aR,4R,6aS)-4-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole-5-carboxylic acid tert-butyl ester

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