1-Methoxycarbonyl-4-formylazulene

Base Information

Chemical Name:1-Methoxycarbonyl-4-formylazulene
CAS No.:43110-60-7
Molecular Formula:C13H10O3
Molecular Weight:214.21700
Hs Code.:
Mol file:43110-60-7.mol

Synonyms:4-Formyl-azulene-1-carboxylic acid methyl ester;4-Formyl-1-methoxycarbonylazulen;4-formyl-1-methoxycarbonylazulene;

Suppliers and Price of 1-Methoxycarbonyl-4-formylazulene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methoxycarbonyl-4-formylazulene

Chemical Property:

PSA：43.37000
LogP:2.39050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Methoxycarbonyl-4-formylazulene

There total 7 articles about 1-Methoxycarbonyl-4-formylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1-methoxycarbonyl-4-(2-(dimethylamino)ethenyl) azulene

: 43110-60-7
4-formyl-1-methoxycarbonylazulene

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1002/anie.200600892

Reference yield: 75.0%

: 43110-66-3
4-hydroxymethyl-1-methoxycarbonylazulene

: 43110-60-7
4-formyl-1-methoxycarbonylazulene

Guidance literature:: With aluminum oxide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/0031-9422(92)83126-J

Reference yield:

: 10527-06-7
1-methoxycarbonyl-4-methylazulene

: 43110-60-7
4-formyl-1-methoxycarbonylazulene

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / dimethylformamide / 1 h / 140 °C

2: 92 percent / sodium periodate / tetrahydrofuran; H₂O / 24 h / 20 °C

With sodium periodate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.200600892