N-(2,5-dichlorophenyl)hydroxylamine

Base Information

• Chemical Name: N-(2,5-dichlorophenyl)hydroxylamine
• CAS No.: 43192-05-8
• Molecular Formula: C6H5Cl2NO
• Molecular Weight: 178.018
• DSSTox Substance ID: DTXSID60530095
• Wikidata: Q82400999
• Mol file: 43192-05-8.mol

Synonyms:43192-05-8;N-(2,5-dichlorophenyl)hydroxylamine;N-(2,5-dichloro-phenyl)-hydroxylamine;2,5-Dichloro-N-hydroxyaniline;SCHEMBL9109201;DTXSID60530095

Chemical Property of N-(2,5-dichlorophenyl)hydroxylamine

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 176.9748192
• Heavy Atom Count: 10
• Complexity: 112

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1Cl)NO)Cl

Technology Process of N-(2,5-dichlorophenyl)hydroxylamine

There total 4 articles about N-(2,5-dichlorophenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,5-dichloronitrobenzene (89-61-2) → N-(2,5-dichloro-phenyl)-hydroxylamine (43192-05-8)

Guidance literature:

With hydrazine hydrate; Raney nickel (type W-4); In ethanol; 1,2-dichloro-ethane; at 10 ℃; for 3h;

DOI:10.1055/s-1984-31027

Reference yield:

2,5-dichloronitrobenzene (89-61-2) → 2,5 dichloroaniline (95-82-9) + N-(2,5-dichloro-phenyl)-hydroxylamine (43192-05-8)

Guidance literature:

With sodium hydrogensulfide; water; calcium chloride;

Reference yield:

2,5-dichloronitrobenzene (89-61-2) → N-(2,5-dichloro-phenyl)-hydroxylamine (43192-05-8)

Guidance literature:

upstream raw materials:

2,5-dichloronitrobenzene

Downstream raw materials:

N-(2,5-Dichlorophenyl)benzohydroxamic acid

N-(2,5-Dichloro-phenyl)-N-hydroxy-acetamide

N-(2,5-dichloro-phenyl)-N-nitroso-hydroxylamin; ammonium salt

bis-(2,5-dichloro-phenyl)-diazene-N-oxide