Carbamic acid, [[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2- azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-, 2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:Carbamic acid, [[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2- azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-, 2-(trimethylsilyl)ethyl ester
CAS No.:433938-50-2
Molecular Formula:C27H32ClF3N4O6Si
Molecular Weight:629.108
Hs Code.:

Carbamic acid,
[[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2-
azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-,
2-(trimethylsilyl)ethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2- azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-, 2-(trimethylsilyl)ethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of Carbamic acid, [[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2- azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-, 2-(trimethylsilyl)ethyl ester

There total 1 articles about Carbamic acid, [[4-[[[[(2S)-1-[(2R)-[3-chloro-5-(trifluoromethoxy)phenyl]hydroxyacetyl]-2- azetidinyl]carbonyl]amino]methyl]phenyl]iminomethyl]-, 2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 433938-49-9
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)OH

: 218598-31-3
H-Aze-Pab(Teoc)

: 433938-50-2
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab-(Teoc)

Guidance literature:: With 2,4,6-trimethyl-pyridine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 20h;

Reference yield: 50.0%

: 35012-55-6
O-pyridin-3-ylmethylhydroxylamine dihydrochloride

: 433938-50-2
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(Teoc)

: 433938-51-3
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(OCH₂-3-pyridine)

Guidance literature:: O-pyridin-3-ylmethylhydroxylamine dihydrochloride; Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(Teoc); In acetonitrile; at 60 ℃;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 46.0%

: 113211-36-2
O-[2-[3-(trifluoromethyl)phenoxy]ethyl]hydroxylamine hydrochloride

: 433938-50-2
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(Teoc)

: 433938-57-9
Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(OCH₂CH₂OPh(3-CF₃))

Guidance literature:: O-[2-[3-(trifluoromethyl)phenoxy]ethyl]hydroxylamine hydrochloride; Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(Teoc); In acetonitrile; at 60 ℃;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;