Propanal, 2-[4-methoxy-5-methyl-2-(1-methylethenyl)phenoxy]-2-methyl-

Base Information

Chemical Name:Propanal, 2-[4-methoxy-5-methyl-2-(1-methylethenyl)phenoxy]-2-methyl-
CAS No.:437650-97-0
Molecular Formula:C15H20O3
Molecular Weight:248.322
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanal, 2-[4-methoxy-5-methyl-2-(1-methylethenyl)phenoxy]-2-methyl-

Chemical Property:

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Technology Process of Propanal, 2-[4-methoxy-5-methyl-2-(1-methylethenyl)phenoxy]-2-methyl-

There total 6 articles about Propanal, 2-[4-methoxy-5-methyl-2-(1-methylethenyl)phenoxy]-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 437650-96-9
2-methyl-2-(2'-isopropenyl-4'-methoxy-5'-methyl phenoxy)propan-1-ol

: 437650-97-0
2-(2-isopropenyl-4-methoxy-5-methyl-phenoxy)-2-methyl-propionaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -68 ℃; for 0.75h;
DOI:10.1039/b200103a

Reference yield:

: 437650-95-8
2-(2-isopropenyl-4-methoxy-5-methyl-phenoxy)-2-methyl-propionic acid

: 437650-97-0
2-(2-isopropenyl-4-methoxy-5-methyl-phenoxy)-2-methyl-propionaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diethyl ether

2: 80 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating

3: 80 percent / oxalyl chloride; dimethyl sulfoxide; triethylamine / CH₂Cl₂ / 0.75 h / -68 °C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane; 3: Swern oxidation;
DOI:10.1016/j.tet.2006.11.014

Reference yield:

: 5248-21-5
4,7-dimethyl-6-methoxy coumarin

: 437650-97-0
2-(2-isopropenyl-4-methoxy-5-methyl-phenoxy)-2-methyl-propionaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent / potassium hydroxide / H₂O; ethane-1,2-diol / 2 h / Heating

2: 70 percent / sodium hydroxide / CHCl₃ / 5 h / Heating

3: 95 percent / diethyl ether

4: 80 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating

5: 80 percent / oxalyl chloride; dimethyl sulfoxide; triethylamine / CH₂Cl₂ / 0.75 h / -68 °C

With potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane; chloroform; water; ethylene glycol; 2: Bargellini reaction / 5: Swern oxidation;
DOI:10.1016/j.tet.2006.11.014