Propanamide, N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl-

Base Information

Chemical Name:Propanamide, N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl-
CAS No.:438608-40-3
Molecular Formula:C36H37N5O5
Molecular Weight:619.72
Hs Code.:

Propanamide,
N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl
methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanamide, N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl-

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Technology Process of Propanamide, N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl-

There total 2 articles about Propanamide, N-[6,9-dihydro-9-[(1S,4R,5S)-5-hydroxy-4-[[(4-methoxyphenyl)diphenyl methoxy]methyl]-2-cyclohexen-1-yl]-6-oxo-1H-purin-2-yl]-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 677757-97-0
N-[9-(5-hydroxy-4-hydroxymethyl-cyclohex-2-enyl)-6-oxo-6,9-dihydro-1H-purin-2-yl]-isobutyramide

: 438608-40-3
N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1016/j.tet.2003.12.052

Reference yield:

: 262372-02-1
(1S,4R,5S)-9-(5-hydroxy-4-hydroxymethyl-2-cyclohexen-1-yl)guanine

: 438608-40-3
N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 1 h / 0 °C

1.2: pyridine / 15 h / 0 - 20 °C

1.3: 730 mg / water / 0.25 h / 20 °C

2.1: 380 mg / pyridine / 0 - 20 °C

With pyridine;
DOI:10.1016/j.tet.2003.12.052