3,4-Dichlorobenzyltriphenylphosphonium chloride

Base Information

Chemical Name:3,4-Dichlorobenzyltriphenylphosphonium chloride
CAS No.:3687-70-5
Molecular Formula:C25H20 Cl2 P . Cl
Molecular Weight:0
Hs Code.:2931900090
NSC Number:71536
UNII:3WM6RS2KA6
DSSTox Substance ID:DTXSID70958069
Wikidata:Q27258149
ChEMBL ID:CHEMBL2005194
Mol file:3687-70-5.mol

Synonyms:Eulan NK;3687-70-5;3,4-Dichlorobenzyltriphenylphosphonium chloride;Eulan NKU;Eulan NK, Eulan NKFW;(3,4-Dichlorobenzyl)triphenylphosphonium chloride;NSC 71536;UNII-3WM6RS2KA6;3WM6RS2KA6;3,4-Dichlorbenzyl-trifenylfosfoniumchlorid [Czech];NSC-71536;Phosphonium, (3,4-dichlorobenzyl)triphenyl-, chloride;(3,4-dichlorophenyl)methyl-triphenylphosphanium chloride;(3,4-dichlorophenyl)methyl-triphenylphosphanium;chloride;3,4-Dichlorbenzyl-trifenylfosfoniumchlorid;Phosphonium, ((3,4-dichlorophenyl)methyl)triphenyl-, chloride;Phosphonium, [(3,4-dichlorophenyl)methyl]triphenyl-, chloride;3-Amino-1-propanesulfonicacid;SCHEMBL7338415;CHEMBL2005194;DTXSID70958069;WLN: GR BG D1PR&R&R &G;LS-106896;Q27258149;3,4-DICHLOROBENZYL-TRIPHENYLPHOSPHONIUM CHLORIDE;[(3,4-Dichlorophenyl)methyl](triphenyl)phosphanium chloride;PHOSPHONIUM, ((3,4-DICHLOROPHENYL)METHYL)TRIPHENYL-, CHLORIDE (1:1)

Suppliers and Price of 3,4-Dichlorobenzyltriphenylphosphonium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
(3,4-Dichlorobenzyl)triphenylphosphoniumchloride 97%
5g
$ 51.33

Total 6 raw suppliers

Chemical Property of 3,4-Dichlorobenzyltriphenylphosphonium chloride

Chemical Property:

PSA：13.59000
LogP:3.49150
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:456.036821
Heavy Atom Count:29
Complexity:418

Purity/Quality:

99% ^*data from raw suppliers

(3,4-Dichlorobenzyl)triphenylphosphoniumchloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[P+](CC2=CC(=C(C=C2)Cl)Cl)(C3=CC=CC=C3)C4=CC=CC=C4.[Cl-]

Technology Process of 3,4-Dichlorobenzyltriphenylphosphonium chloride

There total 4 articles about 3,4-Dichlorobenzyltriphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 102-47-6
3,4-Dichlorophenylmethyl chloride

: 603-35-0
triphenylphosphine

: 3687-70-5
3,4-Dichlorobenzyl-triphenylphosphonium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 3h;
DOI:10.1016/S0960-894X(98)00326-6

Reference yield:

: 1805-32-9
3,4-dichlorobenzyl alcohol

: 3687-70-5
3,4-Dichlorobenzyl-triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / toluene / 0.08 h / Ambient temperature

2: xylene / 22 h / Heating

With thionyl chloride; In toluene; xylene;
DOI:10.1021/jm980572i

Reference yield:

: 6287-38-3
3,4-dichlorobenzaldehyde

: 3687-70-5
3,4-Dichlorobenzyl-triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / Ambient temperature

2: SOCl₂ / toluene / 0.08 h / Ambient temperature

3: xylene / 22 h / Heating

With sodium tetrahydroborate; thionyl chloride; In methanol; toluene; xylene;
DOI:10.1021/jm980572i