(3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran

Base Information

Chemical Name:(3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran
CAS No.:1227-93-6
Molecular Formula:C20H34 O
Molecular Weight:290.489
Hs Code.:
Mol file:1227-93-6.mol

Synonyms:1H-Naphtho[2,1-b]pyran,3-ethenyldodecahydro-3,4a,7,7,10a-pentamethyl-, [3S-(3a,4aa,6ab,10aa,10bb)]-; Labd-14-ene, 8,13-epoxy-, (13S)- (8CI);(+)-13-Epimanoyl oxide; 13-Epimanoyl oxide; 13-epi-Manoyl oxide; Epimanoyloxide

Suppliers and Price of (3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran

Chemical Property:

PSA：9.23000
LogP:5.74280

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran

There total 3 articles about (3S,6aα,10bα)-Dodecahydro-3,4aβ,7,7,10aβ-pentamethyl-3β-vinyl-1H-naphtho[2,1-b]pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 515-03-7
sclareol

: 596-84-9
manoyl oxide

: 564-20-5,1216-84-8,30450-17-0,58976-28-6,64090-92-2,67844-42-2,79768-41-5,79768-42-6,86688-27-9,86688-28-0,95406-08-9,98719-44-9,98719-46-1,131831-65-7,140851-80-5
(3aR)-(+)-sclareolide

: 1227-93-6
(3S,4aR,6aS,10aS,10bR)-3,4a,7,7,10a-Pentamethyl-3-vinyl-dodecahydro-benzo[f]chromene

Guidance literature:: With chromic acid;

Reference yield:

: 515-03-7
sclareol

: 596-84-9
manoyl oxide

: 14506-65-1
15,16-dinor-labd-8-en-13-one

: 909886-71-1
4-((4aS,8aS)-5,5,8a-Trimethyl-2-methylene-decahydro-naphthalen-1-yl)-butan-2-one

: 14699-31-1,24120-97-6,66885-43-6,73610-60-3,126642-09-9
4-((4aS,8aS)-2,5,5,8a-Tetramethyl-1,4,4a,5,6,7,8,8a-octahydro-naphthalen-1-yl)-butan-2-one

: 564-20-5,1216-84-8,30450-17-0,58976-28-6,64090-92-2,67844-42-2,79768-41-5,79768-42-6,86688-27-9,86688-28-0,95406-08-9,98719-44-9,98719-46-1,131831-65-7,140851-80-5
(3aR)-(+)-sclareolide

: 1227-93-6
(3S,4aR,6aS,10aS,10bR)-3,4a,7,7,10a-Pentamethyl-3-vinyl-dodecahydro-benzo[f]chromene

Guidance literature:: With sodium dichromate; sulfuric acid; acetic acid; In water; at 20 ℃; for 36h; Product distribution;

Reference yield:

: 596-85-0
epimanool

: 596-84-9,1227-93-6,19123-29-6,27642-41-7,28235-38-3,28296-72-2,76250-24-3,77171-57-4,77171-58-5
manoyl oxide

: 13β-hydroxylabda-8(17),14-dien-18-oic acid

: 13β-hydroxylabda-8(17),14-dien-18-oic acid methylester

Guidance literature:: Multistep reaction; microbial transformation by Rhodococcus erythropolis JTS-131, 1.) (NH₄)2SO₄, K₂HPO₄, MgSO₄*7H₂O, CaCl₂*2H₂O, FeSO₄*7H₂O, Tween-60, 28 deg C, 12 h 2.) EDTA, 28 deg C, 48 h;