(1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine

Base Information

Chemical Name:(1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine
CAS No.:444798-21-4
Molecular Formula:C28H24N2
Molecular Weight:388.512
Hs Code.:
DSSTox Substance ID:DTXSID00514399
Nikkaji Number:J2.019.466I

Synonyms:444798-21-4;DTXSID00514399;(1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine

Suppliers and Price of (1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine

Chemical Property:

XLogP3:7.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:388.193948774
Heavy Atom Count:30
Complexity:602

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)N=C2C3=CC=CC4=C3C(=CC=C4)C2=NC5=CC(=CC(=C5)C)C)C

Technology Process of (1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine

There total 12 articles about (1Z,2E)-N~1~,N~2~-Bis(3,5-dimethylphenyl)acenaphthylene-1,2-diimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-69-0
3,5-dimethylaminoaniline

: 82-86-0
acenaphthene quinone

: 444798-21-4
α-diimine N,N′-bis(3,5-dimethylphenylimino)acenaphthenequinonate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Reflux;
DOI:10.1016/j.molstruc.2011.02.027

Reference yield:

: C₂₈H₂₄Cl₂N₂Zn

: 444798-21-4
α-diimine N,N′-bis(3,5-dimethylphenylimino)acenaphthenequinonate

Guidance literature:: With potassium carbonate; In water; Reflux;
DOI:10.1021/om501191c

Reference yield:

: 153531-54-5,156398-77-5
N,N'-bis(4-methoxyphenylimino)acenaphthene

: 674322-80-6
[Pd(CH₃)Cl(bis(3,5-(CH₃)2C₆H₃)acenaphthenequinonediimine)]

: 444798-21-4
α-diimine N,N′-bis(3,5-dimethylphenylimino)acenaphthenequinonate

: Pd(Me)Cl(bis(p-MeOC₆H₄-imino)acenaphthene)

Guidance literature:: In chloroform-d1; 1 equiv. of the free ligand was added to a CDCl3 soln. of Pd-complex at 20°C, reaction was monitored by (1)H NMR spectroscopy; equil. const. is given; (1)H NMR spectral data;
DOI:10.1021/om034370i