Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-

Base Information

Chemical Name:Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-
CAS No.:81244-26-0
Molecular Formula:C18H20 N2
Molecular Weight:264.3648
Hs Code.:
DSSTox Substance ID:DTXSID10230977
Wikidata:Q83111764

Synonyms:81244-26-0;Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-;C18H20N;DTXSID10230977;LS-28336

Suppliers and Price of Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-

Chemical Property:

Vapor Pressure:4.94E-08mmHg at 25°C
Boiling Point:442.7°C at 760 mmHg
Flash Point:262.7°C
Density:1.134g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:264.162648646
Heavy Atom Count:20
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C(C3=CC=CC=C3C2NC1)C4=CC=C(C=C4)N
Isomeric SMILES:C1C[C@@H]2[C@@H](C3=CC=CC=C3[C@@H]2NC1)C4=CC=C(C=C4)N

Technology Process of Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)-

There total 9 articles about Benzenamine, 4-(2,3,4,4a,5,9b-hexahydro-1H-indeno(1,2-b)pyridin-5-yl)-, (4a-alpha,5-beta,9b-alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 61490-04-8,81202-63-3
(4aR,5R,9bR)-5-(4-Amino-phenyl)-1,3,4,4a,5,9b-hexahydro-indeno[1,2-b]pyridin-2-one

: 81244-26-0
(4aR,5R,9bR)-4-(2,3,4,4a,5,9b-Hexahydro-1H-indeno[1,2-b]pyridin-5-yl)-phenylamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 6h; Heating;

Reference yield: 48.0%

: 81244-26-0
(4aR,5R,9bR)-4-(2,3,4,4a,5,9b-Hexahydro-1H-indeno[1,2-b]pyridin-5-yl)-phenylamine

: 88763-08-0,107035-06-3,107035-11-0,107035-12-1,81244-26-0
(+/-)-4aS,5R,9bS-5-(4-aminophenyl)-2,3,4,4a,5,9b-hexahydro-1H-indeno<1,2-b>pyridine

Guidance literature:: With potassium hydroxide; In butan-1-ol; for 14h; Heating;

Reference yield:

: 10413-00-0
5-oxo-5-phenylpentanenitrile

: 81244-26-0
(4aR,5R,9bR)-4-(2,3,4,4a,5,9b-Hexahydro-1H-indeno[1,2-b]pyridin-5-yl)-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 85percentiger Phosphorsaeure, Phosphorpentoxid / 1 h / 80 °C

2: 91 percent / hydrogen / Raney-Nickel

3: 75 percent / Lithiumaluminiumhydrid / diethyl ether / 6 h / Heating

With lithium aluminium tetrahydride; phosphoric acid; hydrogen; phosphorus pentoxide; nickel; In diethyl ether;