Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)-

Base Information

Chemical Name:Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)-
CAS No.:457603-47-3
Molecular Formula:C16H21NO2
Molecular Weight:259.348
Hs Code.:
Mol file:457603-47-3.mol

Synonyms:

Suppliers and Price of Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)-

There total 7 articles about Acetic acid, [1-[(1S)-1-phenylethyl]-2-piperidinylidene]-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 121823-95-8
methyl 7-iodohept-2-ynoate

: 457603-47-3
[1-((S)-1-phenylethyl)piperidin-2-ylidene]acetic acid methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium carbonate; sodium iodide; In acetonitrile; for 2h; Heating;
DOI:10.1016/S0040-4039(02)00577-4

Reference yield: 74.0%

: 607388-38-5
{2-[4-((S)-1-phenylethylamino)butyl]-[1,3]dioxolan-2-yl}acetic acid methyl ester

: 457603-47-3
[1-((S)-1-phenylethyl)piperidin-2-ylidene]acetic acid methyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 15h;
DOI:10.1016/S0040-4020(03)00980-3

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 457603-47-3
[1-((S)-1-phenylethyl)piperidin-2-ylidene]acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaI; Na₂CO₃; tetrabutylammonium iodide / acetonitrile / 48 h / Heating

2: 74 percent / BF₃*Et₂O / CH₂Cl₂ / 15 h / 0 °C

With boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; sodium carbonate; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(03)00980-3