Benzenesulfonamide, N-[3-(1,1-dimethylethyl)-3,4-pentadienyl]-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-[3-(1,1-dimethylethyl)-3,4-pentadienyl]-4-methyl-
CAS No.:457630-02-3
Molecular Formula:C16H23NO2S
Molecular Weight:293.43
Hs Code.:

Synonyms:

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Chemical Property of Benzenesulfonamide, N-[3-(1,1-dimethylethyl)-3,4-pentadienyl]-4-methyl-

Chemical Property:

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Technology Process of Benzenesulfonamide, N-[3-(1,1-dimethylethyl)-3,4-pentadienyl]-4-methyl-

There total 6 articles about Benzenesulfonamide, N-[3-(1,1-dimethylethyl)-3,4-pentadienyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 3-tert-butyl-penta-3,4-dienylamine

: 457630-02-3
N-(3-(tert-butyl)-3,4-pentadienyl)-p-toluenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo0342469

Reference yield:

: 55930-38-6
3-(tert-butyl)penta-3,4-dien-1-ol

: 457630-02-3
N-(3-(tert-butyl)-3,4-pentadienyl)-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylazodicarboxilate; triphenylphosphine / toluene; tetrahydrofuran / 0 - 20 °C

2.1: hydrazine hydrate / methanol / 2 h / Heating

2.2: triethylamine / CH₂Cl₂ / 0 - 20 °C

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; toluene; 1.1: Mitsunobi amination;
DOI:10.1002/chem.200600431

Reference yield:

: 52323-98-5
4,4-dimethylpent-2-yn-1-ol

: 457630-02-3
N-(3-(tert-butyl)-3,4-pentadienyl)-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: CH₃COOH / 3 h / 140 °C

2.1: LiAlH₄ / tetrahydrofuran / 0 - 20 °C

3.1: diethylazodicarboxilate; triphenylphosphine / toluene; tetrahydrofuran / 0 - 20 °C

4.1: hydrazine hydrate / methanol / 2 h / Heating

4.2: triethylamine / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; acetic acid; In tetrahydrofuran; methanol; toluene; 1.1: oxy-Cope rearrangement / 3.1: Mitsunobi amination;
DOI:10.1002/chem.200600431