Triethylammonium sulphate (2:1)

Base Information

• Chemical Name: Triethylammonium sulphate (2:1)
• CAS No.: 2399-73-7
• Molecular Formula: C₆H₁₅N*HO₄S
• Molecular Weight: 198.263
• Mol file: 2399-73-7.mol

Synonyms:

Chemical Property of Triethylammonium sulphate (2:1)

Chemical Property:

• Vapor Pressure: 2.07E-07mmHg at 25°C
• Boiling Point: 90.5°Cat760mmHg
• Flash Point: °C
• Density: 0.75g/cm³

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Total 1 MSDS from other Authors

Useful:

Technology Process of Triethylammonium sulphate (2:1)

There total 13 articles about Triethylammonium sulphate (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

triethylamine (121-44-8) → triethylamine sulfate (54272-29-6,27039-85-6,2399-73-7)

Guidance literature:

With sulfuric acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1080/00397910802120916

Reference yield: 96.0%

sulfuric acid (7664-93-9) + triethylamine (121-44-8) → triethylamine sulfate (54272-29-6,27039-85-6,2399-73-7)

Guidance literature:

at 60 - 70 ℃; for 2h;

DOI:10.1080/00397911.2017.1340649

Reference yield:

sulfur dioxide (7446-09-5,12143-17-8,89125-89-3) + triethylamine (121-44-8) → sulphurous acid (7782-99-2) + triethyl ammonium sulphate (27039-85-6,2399-73-7)

Guidance literature:

With H₂O; I₂ or O₂; N(C2H5)3*SO2 formed in absense of H2O and air, then treated with H2O and I2 or O2 of air;

upstream raw materials:

triethylamine

sulfuric acid

Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure

sulfur dioxide

Downstream raw materials:

triethylamine-borane

Refernces

• 1、 Nimbalkar, Urja D.,Seijas, Julio A,Vazquez-Tato, Maria Pilar,Damale, Manoj G,Sangshetti, Jaiprakash N,Nikalje, Anna Pratima G. "Ionic Liquid-catalyzed green protocol for Multi-component synthesis of dihydropyrano[2,3-c]pyrazoles as potential anticancer scaffolds". . . Retrieved 2017.
• 2、 Gschwend, Florence J. V.,Chambon, Clementine L.,Biedka, Marius,Brandt-Talbot, Agnieszka,Fennell, Paul S.,Hallett, Jason P.. "Quantitative glucose release from softwood after pretreatment with low-cost ionic liquids". . p. 692 - 703. Retrieved 2019.
• 3、 Kakati, Praachi,Singh, Preeti,Yadav, Priyanka,Awasthi, Satish Kumar. "Aiding the versatility of simple ammonium ionic liquids by the synthesis of bioactive 1,2,3,4-tetrahydropyrimidine, 2-aminothiazole and quinazolinone derivatives". . p. 6724 - 6738. Retrieved 2021/04/22.
• 4、 -. "ACESULFAME POTASSIUM COMPOSITIONS AND PROCESSES FOR PRODUCING SAME". . . Retrieved 2018/04/13.