2-CYCLOOCTYL-ETHYLAMINE

Base Information

• Chemical Name: 2-CYCLOOCTYL-ETHYLAMINE
• CAS No.: 4744-94-9
• Molecular Formula: C10H21N
• Molecular Weight: 155.28000
• Hs Code.: 2921300090
• Mol file: 4744-94-9.mol

Synonyms:2-cyclooctyl-ethylamine;2-CYCLOOCTYLETHAN-1-AMINE;2-Cyclooctyl-aethylamin;cyclooctylethylamine;

Chemical Property of 2-CYCLOOCTYL-ETHYLAMINE

Chemical Property:

• Vapor Pressure: 0.15mmHg at 25°C
• Boiling Point: 215.1oC at 760 mmHg
• Flash Point: 79.1oC
• PSA: 26.02000
• Density: 0.847g/cm3
• LogP: 3.39600

Purity/Quality:

97% ^*data from raw suppliers

2-Cyclooctylethanamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CYCLOOCTYL-ETHYLAMINE

There total 4 articles about 2-CYCLOOCTYL-ETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(cyanomethyl)cyclooct-1-ene (71750-17-9) → 2-cyclooctylethan-1-amine (4744-94-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;

DOI:10.1021/jm9608671

Reference yield: 67.2%

2-cyclooctylacetonitrile (132557-28-9) → 2-cyclooctylethan-1-amine (4744-94-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 50 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c9cc01330j

Reference yield:

cycloactanone (502-49-8) → 2-cyclooctylethan-1-amine (4744-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate / Erhitzen des Reaktionsprodukts unter vermindertem Druck

2: Raney nickel; ethanolic NH₃ / Hydrogenation

With ammonium acetate; ammonia; nickel;

DOI:10.1021/jo01115a015

upstream raw materials:

(cyanomethyl)cyclooct-1-ene

cycloactanone

2-cyclooctylideneacetonitrile

2-cyclooctylacetonitrile

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