Diphenethylamine, hydrochloride

Base Information

• Chemical Name: Diphenethylamine, hydrochloride
• CAS No.: 6332-28-1
• Molecular Formula: C16H19N
• Molecular Weight: 261.7897
• Mol file: 6332-28-1.mol

Synonyms:NSC 27304;DIPHENETHYLAMINE, HYDROCHLORIDE;Di-(beta-phenylethyl)amine hydrochloride;Benzeneethanamine, N-(2-phenylethyl)-, hydrochloride;N,N-bis(2-phenylethyl)amine hydrochloride;LS-62862

Chemical Property of Diphenethylamine, hydrochloride

Chemical Property:

• Vapor Pressure: 3.61E-05mmHg at 25°C
• Boiling Point: 353.3°Cat760mmHg
• Flash Point: 169.5°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 261.1284273
• Heavy Atom Count: 18
• Complexity: 158

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CC[NH2+]CCC2=CC=CC=C2.[Cl-]

Technology Process of Diphenethylamine, hydrochloride

There total 7 articles about Diphenethylamine, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylacetonitrile (140-29-4) → diphenethyl-amine; hydrochloride (6332-28-1)

Guidance literature:

phenylacetonitrile; With Os(hydride)6(triisopropylphosphine)2; hydrogen; In ⁽²⁾H₈-toluene; at 100 ℃; for 24h; under 3000.3 Torr;

With hydrogenchloride; In water;

DOI:10.1021/acs.organomet.0c00236

Reference yield:

phenylacetonitrile (140-29-4) + cyclohexylamine (108-91-8,157973-60-9) → N-cyclohexyl-2-phenylethylamine hydrochloride (126541-72-8) + diphenethyl-amine; hydrochloride (6332-28-1)

Guidance literature:

phenylacetonitrile; cyclohexylamine; With Os(hydride)6(triisopropylphosphine)2; hydrogen; In ⁽²⁾H₈-toluene; at 100 ℃; for 24h; under 3000.3 Torr;

With hydrogenchloride; In water;

DOI:10.1021/acs.organomet.0c00236

Reference yield:

C21H27NO2 → diphenethyl-amine; hydrochloride (6332-28-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2010.07.003

upstream raw materials:

N-benzylidenebenzylamine

phenylacetaldehyde

phenethylamine

phenylacetonitrile

Downstream raw materials:

C₂₂H₂₀N₃O₇S^(1-)*K⁽¹⁺⁾

Refernces

• 1、 Endeshaw, Molla M.,Li, Catherine,Leon, Jessica De,Yao, Ni,Latibeaudiere, Kirk,Premalatha, Kokku,Morrissette, Naomi,Werbovetz, Karl A.. "Synthesis and evaluation of oryzalin analogs against Toxoplasma gondii". scheme or table. p. 5179 - 5183. Retrieved 2010/10/03.