1,2-Piperidinedicarboxylic acid, 6-propyl-, 2-ethyl 1-(phenylmethyl) ester, (2S,6S)-

Base Information

Chemical Name:1,2-Piperidinedicarboxylic acid, 6-propyl-, 2-ethyl 1-(phenylmethyl) ester, (2S,6S)-
CAS No.:477937-41-0
Molecular Formula:C19H27NO4
Molecular Weight:333.428
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Piperidinedicarboxylic acid, 6-propyl-, 2-ethyl 1-(phenylmethyl) ester, (2S,6S)-

Chemical Property:

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Technology Process of 1,2-Piperidinedicarboxylic acid, 6-propyl-, 2-ethyl 1-(phenylmethyl) ester, (2S,6S)-

There total 7 articles about 1,2-Piperidinedicarboxylic acid, 6-propyl-, 2-ethyl 1-(phenylmethyl) ester, (2S,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5609-09-6
trans 3-hepten-2-one

: 477937-41-0
(2S,6S)-ethyl N-benzyloxycarbonyl-6-propyl-2-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: 94 percent / Triton (R) B / methanol; ethyl acetate / Heating

2.1: 84 percent / p-TSA / toluene / 5 h / Heating

3.1: hydrazine monohydrate / methanol / Heating

4.1: MgSO₄ / CH₂Cl₂ / Heating

4.2: 60 percent / p-TSA / toluene / 3 h / 70 °C

5.1: 92 percent / BF₃*Et₂O / CH₂Cl₂ / 20 h / 20 °C

6.1: H₂ / W₂ Raney nickel / ethanol / 0.5 h / Heating

7.1: Na₂CO₃ / CH₂Cl₂; H₂O / 10 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; N-benzyl-trimethylammonium hydroxide; sodium carbonate; magnesium sulfate; toluene-4-sulfonic acid; hydrazine hydrate; W₂ Raney nickel; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene;

Reference yield:

: 477937-55-6
(+)-(S)-2-(2-aminopentyl)-2-methyl-1,3-dioxane

: 477937-41-0
(2S,6S)-ethyl N-benzyloxycarbonyl-6-propyl-2-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: MgSO₄ / CH₂Cl₂ / Heating

1.2: 60 percent / p-TSA / toluene / 3 h / 70 °C

2.1: 92 percent / BF₃*Et₂O / CH₂Cl₂ / 20 h / 20 °C

3.1: H₂ / W₂ Raney nickel / ethanol / 0.5 h / Heating

4.1: Na₂CO₃ / CH₂Cl₂; H₂O / 10 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; sodium carbonate; magnesium sulfate; W₂ Raney nickel; In ethanol; dichloromethane; water;

Reference yield:

: 477937-40-9
(7S,9S)-7-ethoxycarbonyl-9-propyl-1,4-dithia-8-azaspiro[5.4]decane

: 477937-41-0
(2S,6S)-ethyl N-benzyloxycarbonyl-6-propyl-2-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / W₂ Raney nickel / ethanol / 0.5 h / Heating

2: Na₂CO₃ / CH₂Cl₂; H₂O / 10 h / 20 °C

With hydrogen; sodium carbonate; W₂ Raney nickel; In ethanol; dichloromethane; water;