2-Chloro-3-benzoylquinoxaline

Base Information

Chemical Name:2-Chloro-3-benzoylquinoxaline
CAS No.:49568-79-8
Molecular Formula:C15H9ClN2O
Molecular Weight:268.702
Hs Code.:
DSSTox Substance ID:DTXSID501277039
Nikkaji Number:J406.391K

Synonyms:2-chloro-3-benzoylquinoxaline;SCHEMBL3712426;DTXSID501277039;(3-Chloro-2-quinoxalinyl)phenylmethanone;49568-79-8

Suppliers and Price of 2-Chloro-3-benzoylquinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Chloro-3-benzoylquinoxaline

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:268.0403406
Heavy Atom Count:19
Complexity:330

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2=NC3=CC=CC=C3N=C2Cl

Technology Process of 2-Chloro-3-benzoylquinoxaline

There total 4 articles about 2-Chloro-3-benzoylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 49568-76-5
3-benzoylquinoxalin-2(1H)-one

: 49568-79-8
(3-chloroquinoxalin-2-yl)(phenyl)methanone

Guidance literature:: With trichlorophosphate; at 120 ℃; for 3h;
DOI:10.1039/d0ob01423k

Reference yield: 64.0%

: 1448-87-9
2-chloroquinoxaline

: 611-73-4
Benzoylformic acid

: 49568-79-8
(3-chloroquinoxalin-2-yl)(phenyl)methanone

Guidance literature:: With ammonium peroxydisulfate; iridium(lll) bis[2-(2,4-difluorophenyl)-5-methylpyridine-N,C₂₀]-4,40-di-tert-butyl-2,20-bipyridine hexafluorophosphate; In dimethyl sulfoxide; at 20 ℃; for 12h; regioselective reaction; Inert atmosphere; Irradiation; Green chemistry;
DOI:10.1055/s-0037-1609911

Reference yield:

: 611-73-4
Benzoylformic acid

: 49568-79-8
(3-chloroquinoxalin-2-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: silver nitrate; dipotassium peroxodisulfate / water; acetonitrile / 3 h / 100 °C / Sealed tube

2: thionyl chloride / 2 h / 90 °C

With dipotassium peroxodisulfate; thionyl chloride; silver nitrate; In water; acetonitrile;
DOI:10.1039/c7ob02187a