Phospholane, 1-phenyl-, 1-oxide

Base Information

Chemical Name:Phospholane, 1-phenyl-, 1-oxide
CAS No.:4963-91-1
Molecular Formula:C10H13OP
Molecular Weight:180.186
Hs Code.:
Mol file:4963-91-1.mol

Synonyms:1-oxo-1-phenylphospholane;1-phenylphospholane oxide;1-Phenyl-phospholan-1-oxid;1-Phenyl-phospholane 1-oxide;phenylphospholane oxide;-phenylphospholane 1-oxide;

Suppliers and Price of Phospholane, 1-phenyl-, 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of Phospholane, 1-phenyl-, 1-oxide

Chemical Property:

Melting Point:55 - 57 °C
Boiling Point:136-137 °C(Press: 0.3 Torr)
PSA：26.88000
Density:1.10±0.1 g/cm3(Predicted)
LogP:2.46880

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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MSDS Files:

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Technology Process of Phospholane, 1-phenyl-, 1-oxide

There total 16 articles about Phospholane, 1-phenyl-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 703-03-7
1-phenyl-2-phospholene-1-oxide

: 4963-91-1
1-phenylphospholane-1-oxide

Guidance literature:: With palladium 10% on activated carbon; In methanol; at 20 ℃; for 48h;
DOI:10.1002/chem.201301444

Reference yield: 99.0%

: 5186-73-2
1-phenyl-3-phospholene 1-oxide

: 4963-91-1
1-phenylphospholane-1-oxide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; at 20 ℃; for 48h;
DOI:10.1002/chem.201300546

Reference yield: 75.0%

: 110-52-1
1,4-dibromo-butane

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 4963-91-1
1-phenylphospholane-1-oxide

Guidance literature:: 1,4-dibromo-butane; With magnesium; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

P,P-dichlorophenylphosphine oxide; In tetrahydrofuran; at -78 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/acs.joc.5b01476