5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Base Information

Chemical Name:5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone
CAS No.:111711-98-9
Molecular Formula:C₁₂H₁₃NO₅S
Molecular Weight:283.305
Hs Code.:
DSSTox Substance ID:DTXSID80920550
Nikkaji Number:J423.500B
Mol file:111711-98-9.mol

Synonyms:5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone;111711-98-9;BRN 4755769;2-Pyrrolidinone, 5-(acetyloxy)-1-(phenylsulfonyl)-;SCHEMBL9671729;DTXSID80920550;LS-138592;5-Acetoxy-1-[(phenyl)sulfonyl]pyrrolidin-2-one;1-(BENZENESULFONYL)-5-OXOPYRROLIDIN-2-YL ACETATE

Suppliers and Price of 5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Chemical Property:

Vapor Pressure:2.05E-07mmHg at 25°C
Boiling Point:424.5°C at 760 mmHg
PKA:-15.60±0.40(Predicted)
Flash Point:210.6°C
PSA：89.13000
Density:1.43g/cm³
LogP:1.90560
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:283.05144369
Heavy Atom Count:19
Complexity:461

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1CCC(=O)N1S(=O)(=O)C2=CC=CC=C2

Technology Process of 5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone

There total 3 articles about 5-Acetoxy-1-phenylsulfonyl-2-pyrrolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 108-24-7
acetic anhydride

: 111711-97-8
5-hydroxy-1-phenylsulfonyl-2-pyrrolidinone

: 111711-98-9
5-acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Guidance literature:: for 1.5h; Heating;
DOI:10.1016/0223-5234(91)90101-R

Reference yield:

: 98-10-2
benzenesulfonamide

: 111711-98-9
5-acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus oxychloride / 20 h / Ambient temperature

2: osmium tetraoxide, sodium periodate / dioxane; H₂O / 3 h

3: 72 percent / 1.5 h / Heating

With sodium periodate; osmium(VIII) oxide; trichlorophosphate; In 1,4-dioxane; water;
DOI:10.1016/0223-5234(91)90101-R

Reference yield:

: 111712-01-7
N-benzenesulphonyl-4-pentenoylamide

: 111711-98-9
5-acetoxy-1-phenylsulfonyl-2-pyrrolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: osmium tetraoxide, sodium periodate / dioxane; H₂O / 3 h

2: 72 percent / 1.5 h / Heating

With sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water;
DOI:10.1016/0223-5234(91)90101-R