Phenol, 3-(2-propynyloxy)-, acetate

Base Information

Chemical Name:Phenol, 3-(2-propynyloxy)-, acetate
CAS No.:50584-91-3
Molecular Formula:C11H10O3
Molecular Weight:190.199
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 3-(2-propynyloxy)-, acetate

Chemical Property:

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Technology Process of Phenol, 3-(2-propynyloxy)-, acetate

There total 3 articles about Phenol, 3-(2-propynyloxy)-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3692-88-4
3-hydroxyphenyl propargyl ether

: 108-24-7
acetic anhydride

: 50584-91-3
3-acetoxyphenyl propargyl ether

Guidance literature:: 3-hydroxyphenyl propargyl ether; With dmap; In dichloromethane; at 0 ℃; Inert atmosphere; Cooling with ice;

acetic anhydride; With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jacs.6b11971

Reference yield:

: 108-46-3
recorcinol

: 50584-91-3
3-acetoxyphenyl propargyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / K₂CO₃ / acetone / 22 h / Heating

2: 73 percent / pyridine / CH₂Cl₂ / 5 h / 20 °C

With pyridine; potassium carbonate; In dichloromethane; acetone;
DOI:10.1021/jo015574g

Reference yield:

: 108-46-3
recorcinol

: 50584-91-3
3-acetoxyphenyl propargyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; toluene / 16 h / 60 °C / Sealed tube; Inert atmosphere

2.1: dmap / dichloromethane / 0 °C / Inert atmosphere; Cooling with ice

2.2: 0 - 20 °C / Inert atmosphere

With dmap; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jacs.6b11971