Technology Process of 1,2-Dihydro-1-phenylpyridine
There total 7 articles about 1,2-Dihydro-1-phenylpyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; potassium hydroxide;
In
water;
at 0 - 20 ℃;
for 8h;
Overall yield = 27 mg;
Inert atmosphere;
DOI:10.1002/anie.201810261
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate / acetonitrile / 1.5 h / Sealed tube; Schlenk technique; Inert atmosphere; Irradiation
2: potassium hydroxide; sodium tetrahydroborate / water / 8 h / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; potassium hydroxide;
In
water; acetonitrile;
DOI:10.1002/anie.201810261
- Guidance literature:
-
Multi-step reaction with 3 steps
1: -25 - 20 °C / Inert atmosphere; Sealed tube; Glovebox
2: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate / acetonitrile / 1.5 h / Sealed tube; Schlenk technique; Inert atmosphere; Irradiation
3: potassium hydroxide; sodium tetrahydroborate / water / 8 h / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; potassium hydroxide;
In
water; acetonitrile;
DOI:10.1002/anie.201810261