Diethyl 9h-fluoren-9-yl phosphate

Base Information

Chemical Name:Diethyl 9h-fluoren-9-yl phosphate
CAS No.:34881-01-1
Molecular Formula:C17H19O4P
Molecular Weight:318.309
Hs Code.:
NSC Number:143356
DSSTox Substance ID:DTXSID90301432
Wikidata:Q82045358
Mol file:34881-01-1.mol

Synonyms:diethyl 9h-fluoren-9-yl phosphate;34881-01-1;NSC143356;diethyl9h-fluoren-9-ylphosphate;DTXSID90301432;NSC-143356

Suppliers and Price of Diethyl 9h-fluoren-9-yl phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Diethyl 9h-fluoren-9-yl phosphate

Chemical Property:

Vapor Pressure:1.89E-07mmHg at 25°C
Boiling Point:437.6°Cat760mmHg
Flash Point:231.8°C
Density:1.23g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:318.10209608
Heavy Atom Count:22
Complexity:382

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(OCC)OC1C2=CC=CC=C2C3=CC=CC=C13

Technology Process of Diethyl 9h-fluoren-9-yl phosphate

There total 1 articles about Diethyl 9h-fluoren-9-yl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 486-25-9,952573-42-1
9-fluorenone

: 762-04-9
phosphonic acid diethyl ester

: 100-46-9
benzylamine

: diethyl 9-benzylamino-9H-fluoren-9-yl phosphonate

: 34881-01-1
diethyl 9H-fluoren-9-yl phosphate

: 34881-13-5
diethyl (9-Hydroxy-9H-fluorene-9-yl)phosphonate

Guidance literature:: With magnesium sulfate; tetra(tert-butyl)phthalocyanine aluminum chloride; In dichloromethane; for 72h;
DOI:10.1007/s11172-006-0400-2

Reference yield:

: 34881-01-1
diethyl 9H-fluoren-9-yl phosphate

: 86-73-7
9H-fluorene

: 1530-12-7
9,9'-bifluorenyl

: 2868-70-4
9-ethoxy-fluorenes

: 46880-06-2
N-butyl-9H-fluoren-9-amine

Guidance literature:: With N-butylamine; at 70 ℃; for 12h; Yield given. Further byproducts given. Yields of byproduct given;

Reference yield:

: 34881-01-1
diethyl 9H-fluoren-9-yl phosphate

: 109-73-9,85404-21-3
N-butylamine

: 86-73-7
9H-fluorene

: 3952-42-9
9-butyl-9H-fluorene

: 1530-12-7
9,9'-bifluorenyl

: 46880-06-2
N-butyl-9H-fluoren-9-amine

Guidance literature:: at 70 ℃; for 12h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

upstream raw materials:

9-fluorenone

phosphonic acid diethyl ester

benzylamine

Downstream raw materials:

9H-fluorene

9,9'-bifluorenyl

9-ethoxy-fluorenes

N-butyl-9H-fluoren-9-amine

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