1,3-Bis(ethenyloxy)butane

Base Information

• Chemical Name: 1,3-Bis(ethenyloxy)butane
• CAS No.: 53002-12-3
• Molecular Formula: C8H14O2
• Molecular Weight: 142.198
• DSSTox Substance ID: DTXSID50561373

Synonyms:1,3-Bis(ethenyloxy)butane;53002-12-3;SCHEMBL270010;DTXSID50561373;1,3-butylene glycol divinyl ether

Chemical Property of 1,3-Bis(ethenyloxy)butane

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 142.099379685
• Heavy Atom Count: 10
• Complexity: 99.4

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(CCOC=C)OC=C

Technology Process of 1,3-Bis(ethenyloxy)butane

There total 2 articles about 1,3-Bis(ethenyloxy)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.3%

1.3-butanediol (18826-95-4,107-88-0) + acetylene (74-86-2,25067-58-7) → 2,4-dimethyl-[1,3]dioxane (766-20-1) + 4-vinyloxybutan-2-ol (19255-98-2) + 3-vinyloxybutan-1-ol (103274-69-7) + 1,3-divinyloxybutane (53002-12-3)

Guidance literature:

With potassium hydroxide; at 136 - 140 ℃; for 3h; under 11400 Torr;

DOI:10.1007/BF02498288

Reference yield: 34.0%

1.3-butanediol (18826-95-4,107-88-0) + acetylene (74-86-2,25067-58-7) → 2,4-dimethyl-[1,3]dioxane (766-20-1) + 1,3-divinyloxybutane (53002-12-3)

Guidance literature:

With sodium hydroxide; cesium fluoride; at 140 - 150 ℃; for 2h; under 10297.1 Torr;

DOI:10.1007/s11178-005-0223-x

Reference yield: 97.0%

1,3-divinyloxybutane (53002-12-3) + bis(2-phenylethyl)phosphane sulfide → 2-{3-[2-(diphenethylphosphorothioyl)ethoxy]butoxy}ethyl(diphenethyl)phosphine sulfide (1411984-70-7)

Guidance literature:

In acetonitrile; chemoselective reaction; Inert atmosphere; Irradiation;

DOI:10.1055/s-0032-1316764

upstream raw materials:

1.3-butanediol

acetylene

Downstream raw materials:

2-{3-[2-(diphenethylphosphorothioyl)ethoxy]butoxy}ethyl(diphenethyl)phosphine sulfide

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