1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl-

Base Information

Chemical Name:1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl-
CAS No.:53107-36-1
Molecular Formula:C11H11BrCl2O2
Molecular Weight:326.017
Hs Code.:
Mol file:53107-36-1.mol

Synonyms:2-bromo-2',3'-dichloro-4'-methoxy-isobutyrophenone;2-Brom-2',3'-dichlor-4'-methoxyisobutyrophenon;2Bromo-2',3'-dichloro-4'-methoxyisobutyrophenone;2-bromo-2',3'-dichloro-4'-methoxyisobutyrophenone;2-Bromo-1-(2,3-dichloro-4-methoxy-phenyl)-2-methyl-propan-1-one;

Suppliers and Price of 1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl-

Chemical Property:

Melting Point:72 - 73 °C
Boiling Point:370.0±42.0 °C(Predicted)
PSA：26.30000
Density:1.515±0.06 g/cm3(Predicted)
LogP:4.35820

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl-

There total 2 articles about 1-Propanone, 2-bromo-1-(2,3-dichloro-4-methoxyphenyl)-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 53107-35-0
2',3',-Dichloro-4'-methoxyisobutyrophenone

: 53107-36-1
1-(2,3-dichloro-4-methoxyphenyl)-2-bromo-2-methyl-1-propanone

Guidance literature:: With bromine; In acetic acid; for 16h;
DOI:10.1021/jm00155a038

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 53107-36-1
1-(2,3-dichloro-4-methoxyphenyl)-2-bromo-2-methyl-1-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / AlCl₃ / CH₂Cl₂ / 15 h / Ambient temperature

2: 96 percent / Br₂ / acetic acid / 16 h

With aluminium trichloride; bromine; In dichloromethane; acetic acid;
DOI:10.1021/jm00155a038

Reference yield:

: 53107-36-1
1-(2,3-dichloro-4-methoxyphenyl)-2-bromo-2-methyl-1-propanone

: 57509-50-9,76640-83-0,76640-84-1
6,7-dichloro-2,3-dihydro-5-hydroxy-2-methyl-2-phenyl-1H-inden-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: lithium bromide / N,N-dimethyl-formamide

2: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid

3: potassium tert-butylate / water; tert-butyl alcohol

4: pyridine hydrochloride

With lithium bromide; potassium tert-butylate; pyridine hydrochloride; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid; water; N,N-dimethyl-formamide; tert-butyl alcohol;