cannabielsoin

Base Information

• Chemical Name: cannabielsoin
• CAS No.: 52025-76-0
• Molecular Formula: C₂₁H₃₀O₃
• Molecular Weight: 330.467
• Mol file: 52025-76-0.mol

Synonyms:1,6-Dibenzofurandiol,5a,6,7,8,9,9a-hexahydro-6-methyl-9-(1-methylethenyl)-3-pentyl-, [5aS-(5aa,6a,9a,9aa)]-; Cannabielsoin; CannabielsoinA; Cannabielsoin I

Chemical Property of cannabielsoin

Chemical Property:

• Vapor Pressure: 4.93E-08mmHg at 25°C
• Boiling Point: 426.5°Cat760mmHg
• PKA: 9.78±0.60(Predicted)
• Flash Point: 211.7°C
• Density: 1.089g/cm³

Purity/Quality:

99% ^*data from raw suppliers

CANNABIELSOIN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cannabielsoin

There total 4 articles about cannabielsoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

(1′R,2′R)-5′-methyl-4-pentyl-2′-(prop-1-en-2-yl)-1′,2′,3′,4′-tetrahydro-[1,1′-biphenyl]-2,6-diyl diacetate (40525-15-3) → cannabielsoin (52025-76-0,54002-78-7)

Guidance literature:

With dihydrogen peroxide; potassium hydrogencarbonate; benzonitrile; at 20 ℃; for 40h; Inert atmosphere;

DOI:10.1039/d1cc01971f

Reference yield: 24.0%

CBD (13956-29-1,521-37-9) → cannabielsoin (52025-76-0,54002-78-7)

Guidance literature:

With potassium peroxomonosulfate; In acetone; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1039/d1cc01971f

Reference yield:

→ (5aS,6S,9aR)-9-Isopropenyl-6-methyl-3-pentyl-5a,6,7,8,9,9a-hexahydro-dibenzofuran-1,6-diol (52025-76-0,53969-02-1,112259-07-1,54002-78-7)

Guidance literature:

aus Mischung d. Epoxide 2 u. 3, NaOH;

DOI:10.1021/ja00830a045

upstream raw materials:

CBD

(1′R,2′R)-5′-methyl-4-pentyl-2′-(prop-1-en-2-yl)-1′,2′,3′,4′-tetrahydro-[1,1′-biphenyl]-2,6-diyl diacetate

Downstream raw materials:

dehydrocannabifuran

cannabifuran

Refernces

• 1、 Monroe, Angelina Z.,Gordon, William H.,Wood, Jared S.,Martin, Gary E.,Morgan, Jeremy B.,Williamson, R. Thomas. "Structural revision of a Wnt/β-catenin modulator and confirmation of cannabielsoin constitution and configuration". supporting information. p. 5658 - 5661. Retrieved 2021/06/16.