3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one

Base Information

Chemical Name:3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one
CAS No.:105889-18-7
Molecular Formula:C₁₉H₂₀N₂O₃
Molecular Weight:324.379
Hs Code.:
DSSTox Substance ID:DTXSID70909798

Synonyms:BRN 5613274;2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-;3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one;105889-18-7;DTXSID70909798;LS-98987;3-Benzyl-6-(4-methoxyphenyl)-5,6-dimethyl-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one

Chemical Property:

Vapor Pressure:3.31E-08mmHg at 25°C
Boiling Point:447.6°Cat760mmHg
Flash Point:224.5°C
Density:1.15g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:324.14739250
Heavy Atom Count:24
Complexity:479

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN(C(=O)OC1(C)C2=CC=C(C=C2)OC)CC3=CC=CC=C3

Technology Process of 3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one

There total 3 articles about 3,6-Dihydro-5,6-dimethyl-6-(4-methoxyphenyl)-3-(phenylmethyl)-2H-1,3,4-oxadiazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N'-[2-Hydroxy-2-(4-methoxy-phenyl)-1-methyl-prop-(E)-ylidene]-hydrazinecarboxylic acid methyl ester

: 105889-18-7
3-Benzyl-6-(4-methoxy-phenyl)-5,6-dimethyl-3,6-dihydro-[1,3,4]oxadiazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / benzene; 2-methyl-propan-2-ol / 40 h / Heating

2: 1) NaOEt / 1) EtOH, 12 h RT, 2) EtOH, 48 h, 45 deg C

With potassium tert-butylate; sodium ethanolate; In tert-butyl alcohol; benzene;

Reference yield:

: N'-[2-Hydroxy-2-(4-methoxy-phenyl)-1-methyl-prop-(E)-ylidene]-hydrazinecarboxylic acid ethyl ester

: 105889-18-7
3-Benzyl-6-(4-methoxy-phenyl)-5,6-dimethyl-3,6-dihydro-[1,3,4]oxadiazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / benzene; 2-methyl-propan-2-ol / 40 h / Heating

2: 1) NaOEt / 1) EtOH, 12 h RT, 2) EtOH, 48 h, 45 deg C

With potassium tert-butylate; sodium ethanolate; In tert-butyl alcohol; benzene;