Digermane, 1,1,1-triethyl-2,2,2-triphenyl-

Base Information

Chemical Name:Digermane, 1,1,1-triethyl-2,2,2-triphenyl-
CAS No.:53445-87-7
Molecular Formula:C24H30Ge2
Molecular Weight:463.682
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Digermane, 1,1,1-triethyl-2,2,2-triphenyl-

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Technology Process of Digermane, 1,1,1-triethyl-2,2,2-triphenyl-

There total 4 articles about Digermane, 1,1,1-triethyl-2,2,2-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3005-32-1
triphenylgermanium bromide

: 994-28-5
triethylchlorogermane

: 53445-87-7
1,1,1-triethyl-2,2,2-triphenyldigermane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; (Ar); soln. of SmI2 (2 equiv.) in THF was added to soln. of Et3GeCl and Ph3GeBr (1/1) in hexamethylphosphoric triamide; mixt. was stirred at room temp. for 1 h; chromd. (silica gel, ether); evapd.; chromd. (silica gel, hexane);
DOI:10.1016/j.jorganchem.2004.12.032

Reference yield: 84.0%

: 2816-43-5
triphenylgermane

: 866-37-5
triethylgermyl dimethylamine

: 53445-87-7
1,1,1-triethyl-2,2,2-triphenyldigermane

Guidance literature:: In acetonitrile; byproducts: HNMe2; High Pressure; under inert atm. to soln. Et3GeNMe2 in MeCN soln. Ph3GeH in MeCN was added and heated in tube sealed with Teflon plug at 85°C for 48 h; soln. was allowed to cool, volatiles were removed in vacuo, residue was distilled in Kugelrohr oven (100°C, 0.05 Torr); elem. anal.;
DOI:10.1021/om060115x