Methanone, bis(3,5-dibromophenyl)-

Base Information

Chemical Name:Methanone, bis(3,5-dibromophenyl)-
CAS No.:534591-96-3
Molecular Formula:C13H6Br4O
Molecular Weight:497.806
Hs Code.:
DSSTox Substance ID:DTXSID80468366
Nikkaji Number:J2.718.469C
Wikidata:Q82295539
Mol file:534591-96-3.mol

Synonyms:Methanone, bis(3,5-dibromophenyl)-;534591-96-3;Bis(3,5-dibromophenyl)methanone;bis(3,5-dibromophenyl)ketone;bis(3,5-dibromophenyl) ketone;di(3,5-dibromophenyl)methanone;SCHEMBL1168105;DTXSID80468366;YBIRJZIFQKYQBH-UHFFFAOYSA-N;3,5,3',5'-Tetrabromobenzophenone

Suppliers and Price of Methanone, bis(3,5-dibromophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Methanone, bis(3,5-dibromophenyl)-

Chemical Property:

XLogP3:6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:497.71112
Heavy Atom Count:18
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C=C1Br)Br)C(=O)C2=CC(=CC(=C2)Br)Br

Technology Process of Methanone, bis(3,5-dibromophenyl)-

There total 5 articles about Methanone, bis(3,5-dibromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 160976-68-1
Bis(3,5-dibromophenyl)methanol

: 534591-96-3
3,3',5,5'-(tetrabromo)benzophenone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 1.5h; Molecular sieve;

Reference yield: 58.0%

: 5325-94-0
N-Ethoxycarbonylpiperidine

: 534591-96-3
3,3',5,5'-(tetrabromo)benzophenone

Guidance literature:: 1,3,5-trisbromobenzene; With n-butyllithium; In hexanes; diethyl ether; at -90 ℃;

N-Ethoxycarbonylpiperidine; In hexanes; diethyl ether; at -90 - 20 ℃; Heating / reflux;

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 534591-96-3
3,3',5,5'-(tetrabromo)benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / diethyl ether / 2 h / -78 °C

1.2: 80 percent / diethyl ether / -78 - 20 °C

2.1: 85 percent / oxalylchloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 20 °C

With n-butyllithium; Chloro-oxo-acetic acid; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane; 2.1: Swern oxidation;
DOI:10.1002/ejoc.200500773