9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-
CAS No.:53512-25-7
Molecular Formula:C22H20S
Molecular Weight:316.467
Hs Code.:
DSSTox Substance ID:DTXSID10480839
Nikkaji Number:J2.763.334J
Wikidata:Q82315941
Mol file:53512-25-7.mol

Synonyms:9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-;53512-25-7;DTXSID10480839

Suppliers and Price of 9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:316.12857181
Heavy Atom Count:23
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)C2C3=CC=CC=C3SC4=CC=CC=C24)C

Technology Process of 9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)-

There total 5 articles about 9H-Thioxanthene, 9-(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 90133-31-6
mesityl<2-(phenylthio)phenyl>methanol

: 53512-25-7
9-mesitylthioxanthene

Guidance literature:: With sulfuric acid; for 0.5h; Heating;
DOI:10.1021/jo00187a033

Reference yield: 6.6%

: 90133-47-4
9-mesityl-10-(p-methoxyphenyl)thioxanthenium perchlorate

: 53512-25-7
9-mesitylthioxanthene

: 72780-38-2
9-hydroxy-9-mesitylthioxanthene 10,10-dioxide

: 90133-54-3
9-mesityl-9-(p-methoxyphenyl)thioxanthene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 2h; Further byproducts given; Heating;
DOI:10.1021/jo00187a033

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 53512-25-7
9-mesitylthioxanthene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Mg, (I₂) / diethyl ether / 3 h / Heating

2: 95 percent / H₂SO₄ (80percent) / 0.5 h / Heating

With sulfuric acid; iodine; magnesium; In diethyl ether;
DOI:10.1021/jo00187a033