Technology Process of Benzenepropanethioic acid, S-(1-methylethyl) ester
There total 3 articles about Benzenepropanethioic acid, S-(1-methylethyl) ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diethyl cyanophosphonate; triethylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: [Bu4N][Fe(CO)3(NO)] / 1,4-dioxane / 22 h / 80 °C / Molecular sieve
2: [Bu4N][Fe(CO)3(NO)] / 1,4-dioxane / 24 h / 20 - 80 °C / Molecular sieve; Inert atmosphere
With
[Bu4N][Fe(CO)3(NO)];
In
1,4-dioxane;
DOI:10.1002/chem.201101073
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C
2: [Bu4N][Fe(CO)3(NO)] / 1,4-dioxane / 24 h / 20 - 80 °C / Molecular sieve; Inert atmosphere
With
dmap; dicyclohexyl-carbodiimide;
In
1,4-dioxane; dichloromethane;
DOI:10.1002/chem.201101073
