6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo-

Base Information

Chemical Name:6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo-
CAS No.:53640-81-6
Molecular Formula:C11H15N5O2
Molecular Weight:
Hs Code.:
Mol file:53640-81-6.mol

Synonyms:

Suppliers and Price of 6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo-

There total 6 articles about 6-Pteridinecarboxaldehyde, 2-amino-7,7-diethyl-1,4,7,8-tetrahydro-4-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 52403-64-2
2-amino-6-(1,1-diethyl-3-hydroxy-2-hydroxyiminopropylamino)-5-nitropyrimidin-4(3H)-one

: 52479-24-0
2-amino-7,7-diethyl-7,8-dihydro-6-hydroxymethylpteridin-4(3H)-one

: 53640-81-6
2-amino-7,7-diethyl-4-oxo-3,4,7,8-tetrahydro-pteridine-6-carbaldehyde

Guidance literature:: With sodium hydroxide; sodium dithionite; In water; 1.) reflux;

Reference yield:

: 39821-65-3
1-hydroxy-3-ethylpent-2-ene

: 53640-81-6
2-amino-7,7-diethyl-4-oxo-3,4,7,8-tetrahydro-pteridine-6-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 36 percent / 2-pentyl nitrite, conc. hydrochloric acid / acetic acid / ice-salt bath 30 min, -78 deg C, 10 min

2: 46 percent / methanol sat. with ammonia / 3 days, r.t., 1.5 h, reflux

3: 30 percent / triethylamine / ethanol / 7 h / Heating

4: 3 percent / 0.1M-sodium hydroxide, sodium dithionite / H₂O / 1.) reflux

With hydrogenchloride; sodium hydroxide; sodium dithionite; 1-methylbutyl nitrite; ammonia; triethylamine; In ethanol; water; acetic acid;

Reference yield:

: 15249-93-1
ethyl 3-ethylpent-2-enoate

: 53640-81-6
2-amino-7,7-diethyl-4-oxo-3,4,7,8-tetrahydro-pteridine-6-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / sodium dihydrobisethoxymethoxyaluminate / diethyl ether; benzene / 0 deg C, r.t., 6 h

2: 36 percent / 2-pentyl nitrite, conc. hydrochloric acid / acetic acid / ice-salt bath 30 min, -78 deg C, 10 min

3: 46 percent / methanol sat. with ammonia / 3 days, r.t., 1.5 h, reflux

4: 30 percent / triethylamine / ethanol / 7 h / Heating

5: 3 percent / 0.1M-sodium hydroxide, sodium dithionite / H₂O / 1.) reflux

With hydrogenchloride; sodium hydroxide; sodium dithionite; 1-methylbutyl nitrite; ammonia; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; ethanol; water; acetic acid; benzene;